Martensitic transformation characteristics and its effect of steel Fe-19Cr-0.2Ni-5Mn-0.2Si under cyclic loading
WANG Hong-zhong1, ZOU Zong-yuan1, LI Yin-xiao2, LIU Dou-dou1, ZHAI Dong-lin1, CHEN Lei1
1. Key Laboratory of Advanced Forging and Stamping Technology and Science of Ministry of Education, Yanshan University, Qinhuangdao 066004, Hebei, China; 2. 91737 Troop of PLA, Qinhuangdao 066004, Hebei, China
Abstract:Transformation induced plasticity(TRIP) duplex stainless steel has great potential for industrial application because of its excellent strength and plasticity and economic efficiency. The effect of martensite transformation during cyclic deformation on cyclic mechanical properties of TRIP duplex stainless steel is the basis of promoting its further development and industrial application. Thus the cyclic properties and transformation characteristics of TRIP duplex stainless steel Fe-19Cr-0.2 Ni-5Mn-0.2Si were studied. The tensile mechanical properties and cyclic softening/hardening properties under symmetrical cyclic loading test with 0.6% strain amplitude of the tested steel were determined by INSTRON test machine,respectively. In the process of cyclic loading,the martensitic transformation was measured by ferrite measuring instrument at different cycles,and the characteristics of martensitic transformation were analyzed. Transmission electron microscopy (TEM) was used to observe the microscopic structures of transformation martensite and dislocation under typical cycles. Furthermore,the mechanism of martensitic transformation and dislocation structure evolution on cyclic softening and hardening properties was studied. The results show that the test steel shows obvious TRIP effect under tensile condition. The martensite transformation rate is fast at the early stage of cycling,and then the transformation rate gradually decreases and tends to zero. Cyclic softening and hardening can be divided into three stages: initial cyclic hardening,cyclic softening and secondary cyclic hardening. The hardening effect caused by the proliferation of dislocations in the two phases plays a leading role in the initial cyclic hardening. The subsequent cyclic softening is dominated by the softening effect caused by the low energy dislocation structure in ferrite. In the secondary cyclic hardening stage,the transformation martensite plays a leading role in the hardening of the material. Although transformation martensite has little effect on the cyclic softening and hardening properties of the tested steel at the early stage of cyclic loading,it has a great effect on the properties at the later stage of cyclic loading.
王宏中, 邹宗园, 李银潇, 刘豆豆, 翟东林, 陈雷. Fe-19Cr-0.2Ni-5Mn-0.2Si在循环加载下的马氏体相变规律及其影响[J]. 钢铁, 2021, 56(12): 119-125.
WANG Hong-zhong, ZOU Zong-yuan, LI Yin-xiao, LIU Dou-dou, ZHAI Dong-lin, CHEN Lei. Martensitic transformation characteristics and its effect of steel Fe-19Cr-0.2Ni-5Mn-0.2Si under cyclic loading[J]. Iron and Steel, 2021, 56(12): 119-125.
[1] 高祥明,裴明德,李国平. 冷轧硬化对超级双相不锈钢S32750析出相的影响[J]. 钢铁,2019,54(9):94.(GAO Xiang-ming,PEI Ming-de,LI Guo-ping. Influence of cold rolling on precipitation of S32750 super duplex stainless steel[J]. Iron and Steel,2019,54(9):94.) [2] Ameri A A H,Brown A D,Ashraf M,et al. An effective pulse-shaping technique for testing stainless steel alloys in a Split-Hopkinson pressure bar[J]. Journal of Dynamic Behavior of Materials,2019,5(1):39. [3] Saenarjhan N,Kang J H,Lee S C,et al. Influence of annealing temperature on deformation behavior of 329LA lean duplex stainless steel[J]. Materials Science and Engineering A,2017,679(2):531. [4] 杨吉春,王军,任磊,等. 铈对S32550双相不锈钢微观组织及冲击性能的影响[J]. 钢铁,2020,55(1):86.(YANG Ji-chun,WANG Jun,REN Lei,et al. Effect of Ce on microstructure and impact properties of S32550 duplex stainless steel[J]. Iron and Steel,2020,55(1):86.) [5] 江来珠,张伟,王治宇. 经济型双相不锈钢的研发进展[J]. 钢铁研究学报,2013,25(4):1.(JIANG Lai-zhu,ZHANG Wei,WANG Zhi-yu. Research and development of lean duplex stainless steels[J]. Journal of Iron and Steel Research,2013,25(4):1.) [6] ZHAO Y,ZHANG W,LIU X,et al. Development of TRIP-Aided lean duplex stainless steel by twin-roll strip casting and its deformation mechanism[J]. Metallurgical and Materials Transactions A,2016,47(12):6292. [7] XU Y,LI W,DU H,et al. Tailoring the metastable reversed austenite from metastable Mn-rich carbides[J]. Acta Materialia,2021,214:116986. [8] 侯晓英,毕永杰,郝亮. 热轧TRIP980钢微观组织及强化机制分析[J]. 钢铁,2019,54(4):63. (HOU Xiao-ying,BI Yong-jie,HAO Liang. Analysis on microstructure and strengthening mechanisms of hot-rolled TRIP980 steel[J]. Iron and Steel,2019,54(4):63.) [9] 李霞,李春诚,王溪刚. 冷轧压下率对TRIP钢组织性能的影响[J]. 轧钢,2020,37(4):43. (LI Xia,LI Chun-cheng,WANG Xi-gang. Effect of cold rolling reduction rate on microstructure and mechanical properties of TRIP steel[J]. Steel Rolling,2020,37(4):43.) [10] 王晓晖,康健,李振垒,等. 等温时间对低硅含铝热轧TRIP钢组织性能的影响[J]. 钢铁,2019,54(5):54. (WANG Xiao-hui,KANG Jian,LI Zhen-lei,et al. Effect of isothermal time on microstructures and mechanical properties in hot rolled TRIP steels with low Si and more Al[J]. Iron and Steel,2019,54(5):54.) [11] 姜英花,邝霜. 热处理工艺对相变诱发塑性钢组织和性能的影响[J]. 上海金属,2018,40(5):52.(JIANG Ying-hua,KUANG Shuang. Effect of heat treatment process on microstructure and mechanical properties of TRIP steel[J]. Shanghai Metals,2018,40(5):52.) [12] 张晓宁,张洪坤,余腾义. 高强TRIP钢焊接工艺及冲击韧性[J]. 轧钢,2015,32(6):15.(ZHANG Xiao-ning,ZHANG Hong-kun,YU Teng-yi. Welding process and impact toughness of high strength TRIP steel[J]. Steel Rolling,2015,32(6):15.) [13] 王涛,张梅,刘仁东,等. 第二脉冲电流对TRIP 980钢板电阻点焊接头显微组织和力学性能的影响[J]. 上海金属,2019,41(5):19.(WANG Tao,ZHANG Mei,LIU Ren-dong,et al. Effect of second pulse currents on microstructure and performances of resistance spot welded joint of TRIP 980 steel sheet[J]. Shanghai Metals,2019,41(5):19.) [14] Lillbacka R,Chai G,Ekh M,et al. Cyclic stress-strain behavior and load sharing in duplex stainless steels:Aspects of modeling and experiments[J]. Acta Materialia,2007,55(16):5359. [15] Alvarez-Armas I,Marinelli M C,Malarria J A. Microstructure associated with crack initiation during low-cycle fatigue in a low nitrogen duplex stainless steel[J]. International Journal of Fatigue,2007,29(4):758. [16] Strubbia R,Herenu S,Marinelli M C,et al. Fatigue damage in coarse-grained lean duplex stainless steels[J]. Materials Science and Engineering A,2016,659(6):47. [17] Krupp U,Alvarez-Armas I. Short fatigue crack propagation during low-cycle,high cycle and very-high-cycle fatigue of duplex steel-An unified approach[J]. International Journal of Fatigue,2014,65(8):78. [18] Baudry G,Pineau A. Influence of strain-induced martensitic transformation on the low-cycle fatigue behavior of a stainless steel[J]. Materials Science and Engineering,1977,28:229. [19] 马筱聪,安子军,陈雷,等. 加载方向对TRIP双相不锈钢板带拉伸性能的影响[J]. 钢铁,2020,55(2):112.(MA Xiao-cong,AN Zi-jun,CHEN Lei,et al. Influence of loading direction on tensile properties of a TRIP-assisted duplex stainless steel sheet[J]. Iron and Steel,2020,55(2):112.) [20] 陈雷,张英杰,李飞,等. 固溶温度对节约型双相不锈钢TRIP/TWIP行为的影响[J]. 钢铁,2017,52(4):55.(CHEN Lei,ZHANG Ying-jie,LI Fei,et al. Effect of solution temperature on TRIP/TWIP behavior of a lean duplex stainless steel[J]. Iron and Steel,2017,52(4):55.) [21] Das A. Cyclic plasticity induced transformation of austenitic stainless steels[J]. Materials Characterization,2019,149:1. [22] Talonen J,Aspegren P,Hnninen H. Comparison of different methods for measuring strain induced α-martensite content in austenitic steels[J]. Metal Science Journal,2004,20(12):1506. [23] LI B,ZHENG Y,SHI S,et al. Cyclic deformation behavior and failure mechanism of S32205 duplex stainless steel under torsional fatigue loadings[J]. Materials Science and Engineering A,2020,786(1):139443. [24] YU D,AN K,CHEN Y,et al. Revealing the cyclic hardening mechanism of an austenitic stainless steel by real-time in situ neutron diffraction[J]. Scripta Materialia,2014,89(3):45. [25] Zhao H,Jr E P,Tong J,et al. Mechanical response and dislocation substructure of a cast austenitic steel under low cycle fatigue at elevated temperatures[J]. Materials Science and Engineering A,2017,703(4):422. [26] CHANG B,ZHANG Z. Cyclic deformation behavior in a nitrogen-alloyed austenitic stainless steel in terms of the evolution of internal stress and microstructure[J]. Materials science and Engineering A,2012,556(30):625. [27] Mateo A,Llanes L,Iturgoyen L,et al. Cyclic stress-strain response and dislocation substructure evolution of a ferrite-austenite stainless steel[J]. Acta Materialia,1996,44(31):1143. [28] Nikulina I,Sawaguchi T,Ogawa K. Effect of γ to ε martensitic transformation on low-cycle fatigue behaviour and fatigue microstructure of Fe-15Mn-10Cr-8Ni-xSi austenitic alloys[J]. Acta Materialia,2016,105:207.