Influence of pre-strain on tensile deformation behavior of TRIP-assisted duplex stainless steel
HAO Shuo1, LI Zhi-guo1, ZHANG Xin1, SHE Jun-feng1, LIU Zhi-lei1, CHEN lei1,2
1. College of Mechanical Engineering, Yanshan University, Qinhuangdao 066004, Hebei, China; 2. National Engineering Research Center for Equipment and Technology of Cold Strip Rolling, Qinhuangdao 066004, Hebei, China
Abstract:Pre-deformation, as a key pretreatment process for serving, is usually used to improve the mechanical properties of metal components. In order to clarify the effect of pre-strain on the mechanical behavior and transformation behavior, a series of quasi-static tensile tests were carried out on INSTRON 8801 to investigate the tensile deformation behavior of a TRIP-assisted duplex stainless steel(DSS) and its dependence on pre-strain. The micro-mechanism was discussed by means of TEM analysis, EBSD analysis and in-situ magnetic measurement. The results showed that a typical “three-stage” hardening characteristic of TRIP-assisted DSS was reflected due to the occurrence of strain-induced martensite transformation (SIMT) of γ→ε→α' during tensile deformation, therefore enhanced work hardening ability and mechanical properties were obtained. The introduction of pre-deformation (unloading) did not change the nucleation and growth mechanism of α' martensite, but influenced the work hardening behavior and the mechanical properties of test steel by changing the martensite transformation kinetics in the subsequent deformation process. With the increase of pre-strain level, the (subsequent) yield stress increased and the elongation A decreased gradually. However, different changing trends were revealed in ultimate tensile strength and total elongation At (At=εEpre +A) with increasing pre-strain level, which was closely related to the difference of martensitic transformation kinetics (i.e. transformation degree and transformation rate) under different deformation conditions.
[1] 孙卿卿,仲红刚,曹欣,等. 节约型双相不锈钢性能与研究状况 [J]. 上海金属,2012,34(4):38.(SUN Qing-qing,ZHONG Hong-gang,CAO Xin,et al. Status on production and research of lean duplex stainless steel[J]. Shanghai Metals,2012,34(4):38.) [2] 刘国平. 节约型双相不锈钢组织演变规律的研究进展[J]. 中国冶金,2017,27(3):1.(LIU Guo-ping. Research progress on microstructure evolution of lean duplex stainless steel[J]. China Metallurgy,2017,27(3):1.) [3] 侯雨阳, 成国光. 铁素体不锈钢铸坯凝固特性及等轴晶率控制[J]. 连铸, 2021 (3): 7. (HOU Yu-yang, CHENG Guo-guang. Solidification characteristics and control measures of equiaxed zone ratio of ferritic stainless steel slab[J].Continuous Casting, 2021 (3): 7.) [4] 王胜利.超级马氏体不锈钢成分、工艺和腐蚀性能的研究进展[J].连铸,2019 (3):23.(WANG Sheng-li. Research progress on composition,process and corrosion properties of super martensitic stainless steels[J]. Continuous Casting, 2019 (3):23.) [5] 李璟宇,成国光,陈兴润,等.含钛超纯铁素体不锈钢水口结瘤机制研究[J].连铸,2019 (2):44.(LI Jing-yu, CHENG Guo-guang, CHEN Xing-run,et al.The formation mechanism of the clogging of submerged entry nozzle of Ti-bearing ultra pure ferrite stainless steel[J]. Continuous Casting, 2019 (2):44.) [6] 吴玖. 00Cr18Ni5Mo3Si2双相不锈钢的性能与应用[J]. 钢铁,1985,20(12):40.(WU Jiu. Properties and application of 00Cr18 Ni5Mo3Si2 dual-phase stainless steel[J]. Iron and Steel,1985,20(12):40.) [7] 吴玖. 钢铁研究总院开发了炼油、化工和石油化工用双相不锈钢[J]. 钢铁,1989,24(4):53.(WU Jiu. General iron and steel research institute developed a variety of dual phase stainless steels for oil refinerypetrol-chemical industries[J]. Iron and Steel,1989,24(4):53.) [8] 乔晓燕,赖承班,陈卓,等.奥氏体化工艺对30Cr13钢淬火后的组织和硬度的影响[J].上海金属,2021,43(5):33.(QIAO Xiao-yan, LAI Cheng-ban, CHEN Zhuo,et al. Effect of austenitizing process on microstructure and hardness of 30Cr13 steel after quenching[J]. Shanghai Metal, 2021,43(5):33.) [9] 翁建寅,彭伟,宁小智,等.高氮无镍奥氏体不锈钢的激光辐照组织[J].上海金属,2020,42(3):21.(WENG Jian-yin,PENG Wei, NING Xiao-zhi, et al. Microstructrue of high-nitrogen nickel-free austenitic stainless steel irradiated by laser[J]. Shanghai Metal, 2020,42(3):21.) [10] Herrera C,Ponge D,Raabe D. Design of a novel Mn-based 1 GPa duplex stainless TRIP steel with 60% ductility by a reduction of austenite stability[J]. Acta Materialia,2011,59:4653. [11] Choi J Y,Ji J H,Hwang S W,et al. TRIP aided deformation of a near-Ni-free, Mn-N bearing duplex stainless steel[J]. Materials Science and Engineering: A,2012,535:32. [12] ZHANG W,HU J. Effect of annealing temperature on transformation induced plasticity effect of a lean duplex stainless steel [J]. Materials Characterization,2013,79:37. [13] GUO B F,ZHANG Q F,CHEN L,et al. Influence of annealing temperature on the strain-hardening behavior of a lean duplex stainless steel[J]. Materials Science and Engineering: A,2018,722:216. [14] 陈雷, 李飞, 张英杰,等. 一种TRIP/TWIP型双相不锈钢的相图及其亚稳奥氏体组织稳定性计算[J]. 燕山大学学报,2016(40):35 (CHEN Lei, LI Fei, ZHANG Ying-jie, et al. Calculation for the phase diagram and stability of metastable austenite in a TRIP/TWIP duplex stainless steel[J]. Jouranl of Yanshan University,2016(40): 35.) [15] Choi J Y,Ji J H,Hwang S W,et al. Effects of nitrogen content on TRIP of Fe-20Cr-5Mn-xN duplex stainless steel[J]. Materials Science and Engineering: A,2012,534:673. [16] Tsuchida N,Yamaguchi Y,Morimoto Y,et al. Effects of temperature and strain rate on TRIP effect in SUS301L metastable austenitic stainless steel[J]. ISIJ International,2013,53(10):1881. [17] 陈雷, 郝硕, 梅瑞雪,等. 节约型双相不锈钢TRIP效应致塑性增量及其固溶温度依赖性 [J]. 金属学报,2019, 55(11):1359.(CHEN Lei,HAO Shou,MEI Rei-xue,et al. Intrinsic increment of plasticity induced by TRIP and its dependence on the annealing temperature in a lean duplex stainless steel[J]. Acta Metallurgica Sinica,2019,55(11):1359.) [18] Lechartier A,Meyer N,Estevez R,et al. Deformation behavior of lean duplex stainless steels with strain induced martensitic transformation: Role of deformation mechanisms, alloy chemistry and predeformation[J]. Materialia,2019,5:100190. [19] PENG J,LI K S,PEI J F,et al. The effect of pre-strain on tensile behaviour of 316L austenitic stainless steel[J]. Materials Science and Technology,2018,34(5):547. [20] PENG J,LI K S,DAI Q,et al. Mechanical properties of pre-strained austenitic stainless steel from the view of energy density[J]. Results in Physics,2018,10:187. [21] LI S H,DAN W J,ZHANG W G,et al. A model for strain-induced martensitic transformation of TRIP steel with pre-strain[J]. Computational Materials Science,2008, 40(2):292. [22] 徐勇, 张士宏, 程明,等. 加载方式对奥氏体不锈钢力学性能和马氏体相变的影响 [J]. 金属学报,2013,49(7):775. (XU Yong,ZHANG Shi-hong,CHENG Ming,et al. Effect of loading modes on mechanical property and strain induced martensite transformation of austenitic stainless steels[J]. Acta Metallurgica Sinica,2013,49(7):775.) [23] Joshua A L,Chester J V T,Martin C M. Effect of strain rate on stress-strain behavior of alloy 309 and 304L austenitic stainless steel[J]. Metallurgical and Materials Transactions:A,2006,37(1):147. [24] Dieter G E. Mechanical Metallurgy[M]. New York: McGraw Hill Book Company,1988. [25] Talonen J,Aspegren P,Hnninen H. Comparison of different methods for measuring strain induced α'-martensite content in austenitic steels[J]. Materials Science and Technology,2004,20(12):1506. [26] 陈雷,张英杰,李飞,等. 固溶温度对节约型双相不锈钢TRIP/TWIP行为的影响[J]. 钢铁,2017,52(4):55.(CHEN Lei,ZHANG Ying-jie,LI Fei,et al. Effect of solution temperature on the TRIP+TWIP behavior of the lean duplex stainless steel[J]. Iron and Steel,2017,52(4):55.) [27] Choi J Y,Ji J H,Hwang S W,et al. Strain induced martensitic transformation of Fe-20Cr-5Mn-0.2Ni duplex stainless steel during cold rolling:Effects of nitrogen addition[J]. Materials Science and Engineering: A,2011,528(18):6012. [28] 胡汉江,赵爱民,印珠凯,等. 预应变对TRIP钢力学性能及硬化行为的影响 [J]. 材料热处理学报,2016,37(5):128. (HU Han-jiang,ZHAO Ai-min,YIN Zhu-kai,et al. Effect of pre-strain on mechanical properties and hardening behavior of TRIP steel[J]. Journal of Materials Heat Treatment,2016,37(5):128.) [29] LI X F,LI J J,DING W,et al. Stress relaxation in tensile deformation of 304 stainless steel[J]. Journal of Materials Engineering and Performance,2017,26(2):630. [30] LIU H P,LIU B,BAI P K,et al. Martensitic transformation and fractographic analysis of lean duplex stainless steel during low temperature tension deformation[J]. Materials Characterization,2015,107:262. [31] Wibowo F,Zulfi F R,Korda A,et al. Effect of tensile pre-strain at different orientation on martensitic transformation and mechanical properties of 316L stainless steel[J]. AIP Conference Proceedings,2017,1805(1):1. [32] Breedis J F. Influence of dislocation substructure on the martensitic transformation in stainless steel[J]. Acta Metallurgica,1965,13(3):239. [33] ZHAO Y,WANGY,LI X,et al. Effects of plastic straining on the corrosion resistance of TRIP-aided lean duplex stainless steels[J]. Journal of Materials Science,2018,53(12):9258. [34] XU Y,ZHANG S H,CHENG M,et al. In situ X-ray diffraction study of martensitic transformation in austenitic stainless steel during cyclic tensile loading and unloading[J]. Scripta Materialia,2012,67(9):771. [35] Spencer K K,Véron M,Zhang Y,et al. The strain induced martensite transformation in austenitic stainless steels Part 1-influence of temperature and strain history[J]. Materials Science and Technology,2009,25(1):7. [36] XU Y,ZHANG S H,SONG H W,et al. The enhancement of transformation induced plasticity effect on austenitic stainless steels by cyclic tensile loading and unloading[J]. Materials Letters,2011,65(11):1545. [37] 金淼, 李文权, 郝硕,等. 固溶温度对Mn-N型双相不锈钢拉伸变形行为的影响 [J]. 金属学报,2019,55(4):436.(JIN Miao,LI Wen-quan,HAO Shuo,et al. Effect of solution temperature on tensile deformation behavior of Mn-N bearing duplex stainless steel[J]. Acta Metallurgica Sinica,2019,55(4):436.) [38] 马筱聪,安子军,陈雷,等. 加载方向对TRIP双相不锈钢板带拉伸性能的影响[J]. 钢铁,2020,55(2):112.(MA Xiao-cong,AN Zi-jun,CHEN Lei,et al. Influence of loading direction on tensile properties of a TRIP-assisted duplex stainless steel sheet[J]. Iron and Steel,2020,55(2):112.)