|
|
|
| Sintering kinetics involving grain growth and densification of Mg-PSZ nanopowders |
| Yi-ming She1, Jie-fu Lang1,2, Di An3, Chao-wei Si1, Xu-dong Luo1,3, Zhi-peng Xie3, Jie-gang You1 |
1 School of Materials and Metallurgy, University of Science and Technology Liaoning, Anshan 114051, Liaoning, China
2 Institute of Advanced Structures, Beijing Institute of Technology, Beijing 100081, China
3 State Key Lab of New Ceramics and Fine Processing, School of Materials Science and Engineering, Tsinghua University, Beijing 100084, China |
|
|
|
|
Abstract Sintering kinetics have been found to be effective in judging the evolution of ceramics. By using magnesium oxide-partially stabilized zirconia (Mg-PSZ) powder prepared by co-precipitation as raw materials, the evolution of densification and grain growth for Mg-PSZ ceramics were investigated. The results indicated that the densification of samples was mainly controlled by grain boundary diffusion in intermediate sintering stage. During the sintering process, the grain growth mechanisms included normal grain growth, abnormal grain growth and solid solution drag-controlled grain growth. Interestingly, the apparent activation energy for grain growth of Mg-PSZ ceramics is lower than that of ZrO2–Y2O3 ceramics in the solid solution drag-controlled grain grow process, which will cause grain to grow easily. The sintering kinetics and microstructure of Mg-PSZ ceramics were studied, and the kinetic equation of grain growth at different temperatures was established. The results show that the strength difference between Mg-PSZ and yttrium oxide-stabilized zirconia is closely related to the easy grain growth of Mg-PSZ ceramics.
|
|
Received: 02 September 2021
Published: 25 July 2022
|
|
|
|
| Cite this article: |
|
Yi-ming She,Jie-fu Lang,Di An, et al. Sintering kinetics involving grain growth and densification of Mg-PSZ nanopowders[J]. Journal of Iron and Steel Research International, 2022, 29(7): 1138-1144.
|
|
|
|
| [1] |
ZHAO Tongxin，YOSHIMI Satoshi，SUN Youbao，HUANG Taohong. Application of electron probe microanalysis (EPMA) in characterization of neodymiumironboron (NdFeB) magnetic materials[J]. PHYSICS EXAMINATION AND TESTING, 2022, 40(1): 20-. |
| [2] |
ZHANG Xian-wei1,2,ZHANG Hong-wei1,2,LEI Hong1,2,WANG Qiang1,2. Simulation of divorced eutectic microstructure evolution in ductile iron solidification process[J]. JOURNAL OF IRON AND STEEL RESEARCH , 2020, 32(9): 816-825. |
| [3] |
ZHENG Hong-guang, LIU Hua-song. Grain coarsening of As-cast austenite and evolution of grain structure during hot charging reheating[J]. CONTINUOUS CASTING, 2020, 39(2): 45-51. |
| [4] |
ZHAOTong-xin. Electron probe microanalyzer characterization for grain boundary diffusion of terbium into sintered Nd-Fe-B material[J]. PHYSICS EXAMINATION AND TESTING, 2019, 37(2): 20-22. |
|
|
|
|
2022, Vol. 29 
