Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography

Jian Zhu, Zhi-hao Zhang, Jian-xin Xie

钢铁研究学报(英文版) ›› 2021, Vol. 28 ›› Issue (10) : 1268-1281.

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钢铁研究学报(英文版) ›› 2021, Vol. 28 ›› Issue (10) : 1268-1281. DOI: 10.1007/s42243-021-00595-1
论著

Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography

  • Jian Zhu1, Zhi-hao Zhang1,2, Jian-xin Xie1,2
作者信息 +

Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography

  • Jian Zhu1, Zhi-hao Zhang1,2, Jian-xin Xie1,2
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摘要

Based on the parent austenite orientation reconstruction method, it is aimed to reveal the origination of high angle grain boundaries (HAGBs) and its relationship with ductility of H13 steel. The orientation relationship between martensite andparent austenite of quenched H13 samples was (123.5°, 9.3°, 192.5°), which agreed with the Kurdumov–Sachs relationship.The variant distribution of quenched samples was dominated by close-packed plane group, and its high length fraction ofV1/V2 inter-variant boundaries of calculated 62.6% was mainly contributed to HAGBs (>45°). When the quenched H13samples underwent the pre-tempering treatment, their density of HAGBs (>45°) notably increased from 1.33 to 2.39l m-1, which improved its total elongation from 8.3% to 11.5%. Compared with the quenched H13 samples, the length fraction of V1/V2 inter-variant boundaries of H13 samples with pre-tempering for 5, 10 and 60 min was reduced by 6.7%,7.0% and 7.5%, respectively. During pre-tempering treatment, V1/V3&V5 variant pairs, etc., merged V1/V2 variant pairby strain-induced grain boundary migration, which decreased the length fraction of V1/V2 inter-variant boundaries by7.0%. The pre-tempering treatment significantly increased HAGBs (>45°) of H13 samples by sub-grains coarsening andstrain-induced grain boundary migration mechanism.

Abstract

Based on the parent austenite orientation reconstruction method, it is aimed to reveal the origination of high angle grain boundaries (HAGBs) and its relationship with ductility of H13 steel. The orientation relationship between martensite andparent austenite of quenched H13 samples was (123.5°, 9.3°, 192.5°), which agreed with the Kurdumov–Sachs relationship.The variant distribution of quenched samples was dominated by close-packed plane group, and its high length fraction ofV1/V2 inter-variant boundaries of calculated 62.6% was mainly contributed to HAGBs (>45°). When the quenched H13samples underwent the pre-tempering treatment, their density of HAGBs (>45°) notably increased from 1.33 to 2.39l m-1, which improved its total elongation from 8.3% to 11.5%. Compared with the quenched H13 samples, the length fraction of V1/V2 inter-variant boundaries of H13 samples with pre-tempering for 5, 10 and 60 min was reduced by 6.7%,7.0% and 7.5%, respectively. During pre-tempering treatment, V1/V3&V5 variant pairs, etc., merged V1/V2 variant pairby strain-induced grain boundary migration, which decreased the length fraction of V1/V2 inter-variant boundaries by7.0%. The pre-tempering treatment significantly increased HAGBs (>45°) of H13 samples by sub-grains coarsening andstrain-induced grain boundary migration mechanism.

关键词

Variant selection / High angle grain boundary / Parent austenite orientation reconstruction / Pre-tempering treatment / H13 steel

Key words

Variant selection / Pre-tempering treatment / Parent austenite orientation reconstruction / High angle grain boundary / H13 steel

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Jian-xin Xie, Zhi-hao Zhang, Jian Zhu. Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography[J]. 钢铁研究学报(英文版), 2021, 28(10): 1268-1281 https://doi.org/10.1007/s42243-021-00595-1
Jian-xin Xie, Zhi-hao Zhang, Jian Zhu. Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography[J]. Journal of Iron and Steel Research International, 2021, 28(10): 1268-1281 https://doi.org/10.1007/s42243-021-00595-1

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