2012年, 第19卷, 第10期　刊出日期：2012-10-15

  

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工艺
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  Effects of Temperature and Atmosphere on Sintering Process of Iron Ores

  ZHANG Jun,GUO Xing-min,HUANG Xue-jun

  中国钢铁期刊网. 2012, 19(10): 1-6.

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  The relationship of time to minerals composition in sinters is investigated by mineragraphy are claritied observation and component analysis, and the effects of temperature and atmosphere on mineralization process. Results are obtained as follows. The initial melt forms below the eutectic temperature of CaO·Fe2O3 and CaO·2Fe2O3, which is complex substance containing Ca, Fe, Si and Al, rather than the binary calcium ferrite melt. Minerals composition of binding phase is related to local content of silica in melt, which is influenced by temperature. Appearance of the melt promotes the transition from hematite to magnetite, which then alters the mechanism of calcium ferrite formation. Before the formation of magnetite, the contents of Fe and Ca within the multiple calcium ferrite decrease with temperature, but in the case of magnetite presence, the content of Fe increases solely with increase of temperature and decrease of oxygen potential. Temperature and atmosphere determine minerals composition together, and bring influence on sintering process in different ways. It can be deduced that temperature affects kinetics of the mineralization process, but atmosphere just plays a role in thermodynamics.
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  Effects of Temperature and Atmosphere on Pellets Reduction Swelling Index

  WANG Zhao-cai,CHU Man-sheng,LIU Zheng-gen,CHEN Shuang-yin,XUE Xiang-xin

  中国钢铁期刊网. 2012, 19(10): 7-12.

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  After taking into account the conditions of the domestic iron resources and the non-coking coal resources, the process of coal gasification-shaft furnace is an effective way to develop direct reduction iron in China. The following tasks are very critical to choose suitable process of shaft furnace and gasification, including the production of oxidized pellets with excellent comprehensive properties as well as the study of the reaction behavior and mechanism of swelling. The results showed that the oxidized pellets of using domestic magnetic iron concentrate as raw materials have favorable comprehensive properties, including higher mechanical strength both before and after reduction, faster reduction rate and lower reduction swelling index (RSI). All of these properties can meet the shaft furnace yielding requirement. When the temperature was below 1223 K, the pellets′ RSI was lower than 20%. With increasing of the content of H2 in atmosphere, the pellets reaction rate accelerated, crushing strength enhanced and RSI decreased. The RSI dropped to 10.26% at 1323 K in 100% H2 atmosphere, and it is up to 39.88% in 100% CO atmosphere. The iron grains mainly presented in platelike when pellets were reduced by H2, however, in CO atmosphere the iron grains were precipitated in flocculent. The whisker shape of iron grains and heating effects of reduction reaction are the major factors leading to the poor pellets strength and increase of RSI. Appropriately controlling the temperature and increasing the ratio of H2 to CO in atmosphere are good for dropping the RSI.
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  HCWCI/Carbon Steel Bimetal Liner by Liquid-Liquid Compound Lost Foam Casting

  XIAO Xiao-feng,,YE Sheng-ping,YIN Wei-xin,XUE Qiong4

  中国钢铁期刊网. 2012, 19(10): 13-19.

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  Impact, friction and corrosion from the grinding balls and the grinding medium during the mineral processing result in liner breakage. Liner, made from Hadfield steel or alloyed steel, could not have served in wet grinding environment for more than ten months. Composite liner, made from HCWCI (high Cr white cast iron) and carbon steel, has been developed successfully with liquid-liquid composing process based on LFC (lost foam casting). The microstructure of composite was analyzed with optical microscope, SEM (scanning electron microscope)/EDX energy-dispersive X-ray and XRD (X-ray diffraction). According to micrograph, the combination region of two metals was staggered like dogtooth, no mixtures occurred between two liquid metals, and its interface presented excellent metallurgical bonding state. The results of mechanical property test show that, the hardness of HRC, the fracture toughness, and the bending strength are more than 61, 16.5 J/cm2 and 1600 MPa, respectively. Comparison between liners made from bimetal composite and alloyed steel has also been investigated in industrial hematite ball mill. The results of eight months test in wet grinding environment prove that the service life of bimetal composite liner is three times as long as that of one made from alloyed steel.
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  Tension and Thickness Control Strategy Analysis of Two Stands Reversible Cold Rolling Mill

  LIU Guang-ming,DI Hong-shuang,ZHOU Cun-long,LI Hong-cui,LIU Jiang

  中国钢铁期刊网. 2012, 19(10): 20-25.

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  In order to lucubrate the rolling characteristic of the two stands reversible cold rolling mill and establish the tension and thickness control strategy, the steady-state characteristic simulating program was established using the steady-state continuous rolling theory. The influences of each factor on exit thickness under different tension control methods were analyzed. The results show that, the influence of the entry stand gap on exit thickness is significant and it changes little with different tension control methods. As a result, the entry stand gap can be used as the main control method of exit thickness, whereas rolling speed of any stand and roll gap of the exit stand can be used to adjust the inter-stand tension. The results are beneficial for thickness and tension control of the two stands reversible cold rolling mill.
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  Finite Element Method Analysis of Effect of Blade Clearance on Plate Shearing Process

  LI Yu-gui,YE Quan,FAN Fei,BAO Ye,HUANG Qing-xue

  中国钢铁期刊网. 2012, 19(10): 26-29.

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  Blade clearance is an important technical parameter of the shear, which determines the shear quality of plate. The finite element method was used to simulate shearing process which is in the different specifications and blade clearances, and the impact on blade section and shearing force of blade clearance was analyzed. Comparing with traditional experience formulas and measured values, the limitations of the experience formulas were proved. And by contrasting with the shearing force data collected from Linfen Iron and Steel Company, the reliability of the finite element method was further proved. The simulated results show that the simulated values controlled by ductile fracture criterion and measured values are very close, and the deviation value is in the range of 4.8%-20.8%. For the same steel, if the plate is thicker, the blade clearance will be greater, and thickness and blade clearance are approximately linear. The difference between numerical simulation of the maximum shearing force and the measured results is 7.7% to 12.0%, and the simulation results are close to facts. With the increase of blade clearance and the thickness, the shearing force was increased to some degree.
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  Investigation on Co-Combustion Kinetics of Anthracite and Waste Plastics by Thermogravimetric Analysis

  LIU Zheng-jian,REN Shan,ZHANG Jian-liang,LIU Wei-jian,XING Xiang-dong,SU Bu-xin

  中国钢铁期刊网. 2012, 19(10): 30-35.

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  In order to effectively recycle resource for the benefit of the global environment, the utilization of waste plastics as auxiliary injectant for blast furnaces is becoming increasingly important. Combustion kinetics of plastics-coal blends with 0, 10%, 20% and 40% waste plastics (WP) are investigated separately by thermogravimetric analysis (TGA) from ambient temperature to 900 ℃ in air atmosphere. These blends are combusted at the heating rates of 5, 10 and 20 ℃/min. The results indicate that, with the increase of waste plastics content, the combustion processes of blends could be divided into one stage, two stages and three stages. The waste plastics content and heating rates have important effects on the main combustion processes of blends. With the increase of waste plastics content, the ignition temperature and the final combustion temperature of blends tend to decrease, while the combustion reaction becomes fiercer. With the increase of the heating rate, the ignition temperature, the mass loss rate of the peaks and the final combustion temperature of blends combustion tend to increase. The Flynn-Wall-Ozawa (FWO) iso-conversional method is used for the kinetic analysis of the main combustion process. The results indicate that, when the waste plastics content varied from 0 to 40%, the values of activation energy increase from 126.05 to 184.12 kJ /mol.
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  Effects of Oxides Contents in Vanadium Slag on Corrosion Mechanism of MgO-C Bricks

  WANG Guang-en,WANG Yu,XIE Bing,LI Xin-sheng,GUO Xu,LI Xiao-jun

  中国钢铁期刊网. 2012, 19(10): 36-42.

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  The influence of V2O3, FeO, TiO2, MnO and MgO in vanadium slag on the corrosion mechanism of MgO-C bricks was studied by stationary immersion tests at vanadium-extracting temperature. Experimental results show that FeO, TiO2, and MnO could enhance the corrosion rate and V2O3 and MgO could decrease it. Microstructure and phase composition of worn samples were investigated by SEM-EDS, revealing the presence of Fe particles, produced by graphite reduction, and (Mg,Fe,Mn)O solid solution at the interface. The formation process of (Mg,Fe,Mn)O solid solution was discussed and the corrosion mechnism of MgO-C bricks was thus proposed.
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  Effect of Sinter Hardening on Microstructure and Mechanical Properties of Astaloy 85Mo

  K Sheikhi Moghaddam,M Ghambari,H Farhangi,N Solimanjad

  中国钢铁期刊网. 2012, 19(10): 43-46.

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  Effect of sinter hardening on the microstructure, density, hardness and tensile properties of Astaloy 85Mo+0.7% graphite was investigated. For this purpose, Astaloy 85Mo, a pre-alloyed powder, was mixed with 0.7% UF4 graphite and then pressed in single action die and sintered at 1120 ℃ for 30 min in N2-10%H2 atmosphere. Then samples were cooled from 0.5 to 3 ℃/s sintering temperature in accordance with different cooling rates. The difference in microstructure, hardness, density and tensile properties of the samples associated with different cooling rates from sintering temperature has been investigated. The results show that the microstructure remains bainitic by changing cooling rate, but it becomes finer and then the hardness and tensile strength of the samples will increase by increasing the cooling rate from sintering temperature.
材料
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  Energy-Based Prediction of Low Cycle Fatigue Life of High-Strength Structural Steel

  LUO Yun-rong,,HUANG Chong-xiang,GUO Yi,WANG Qing-yuan

  中国钢铁期刊网. 2012, 19(10): 47-53.

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  Energy-based models for predicting the low-cycle fatigue life of high-strength structural steels are presented. The models are based on energy dissipation during average of cycles, cycles to crack propagation and total cycles to failure. Plastic strain energy per cycle was determined and found as an important characteristic for initiation and propagation of fatigue cracks for high-strength structural steels. Fatigue strain-life curves were generated using plastic energy dissipation per cycle (loop area) and compared with the Coffin-Manson relation. Low cycle fatigue life was found similar from both methods. The material showed Masing-type behavior. The cyclic hysterisis energy per cycle was calculated from cyclic stress-strain parameters. The fracture surfaces of the fatigue samples were characterized by scanning electron microscope and the fracture mechanisms were discussed.
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  Finite Element Analysis of Die Geometry and Process Conditions Effects on Equal Channel Angular Extrusion for β-Titanium Alloy

  SI Jia-yong,,GAO Fan,ZHANG Ji

  中国钢铁期刊网. 2012, 19(10): 54-58.

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  The finite element analysis was applied to evaluate the respective influences of die geometry and process conditions on plastic strain distribution for β-titanium (Ti-13V11Cr3Al) alloy during the equal channel angular extrusion (ECAE). It was found that optimum equal channel angular extrusion die geometry is strongly material dependent. Optimal strain homogeneity in the Ti-13V11Cr3Al alloy may be achieved at r (inner radius)=5 mm, R (outer radius)=3 mm. The equivalent plastic strain increases with increasing friction coefficient. And the better homogeneity of the equivalent plastic strain distribution can be achieved when friction coefficient value is lower. The faster the ram speed is, the lower the homogeneity of the equivalent plastic strain distribution is and the influence is slight. The back-pressure does not help to improve the plastic strain homogeneity, and the increasing temperature has a slightly favourable effect on the plastic strain homogeneity between 400 and 600 ℃.
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  Effect of Cold Rolling on Microstructure and Mechanical Properties of AISI 301LN Metastable Austenitic Stainless Steels

  HUANG Jun-xia,YE Xiao-ning,XU Zhou

  中国钢铁期刊网. 2012, 19(10): 59-63.

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  The microstructure and mechanical properties evolution of AISI 301LN metastable austenitic stainless steels during cold rolling were investigated. A wide range of cold thickness reduction (10%-80%) was carried out in a four-high rolling mill at ambient temperature. The X-ray and Feritscope MP30 were used to identify the strain-induced α′-martensite phase and its volume fraction, respectively. The microstructure was observed by optical micrograph and the mechanical properties were determined by tensile tests and microhardness. The results show that the strain-induced α′-martensite nucleated at the shear bands intersections and the growth of α′-martensite occurred by the repeated nucleation of new embryos. The volume fraction of strain-induced α′-martensite increased with increasing the cold rolling reduction. In addition, the percentage increased in the tensile strength is the same as that of hardness. The ratio between the average tensile strength and the average microhardness was found to range between 2.82 and 3.17.
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  Influence of Rotational Speed on Microstructure and Mechanical Properties of Dissimilar Metal AISI 304-AISI 4140 Continuous Drive Friction Welds

  G Subhash Chander,G Madhusudhan Reddy,A Venugopal Rao

  中国钢铁期刊网. 2012, 19(10): 64-73.

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  Fundamental investigation of continuous drive friction welding of austenitic stainless steel (AISI 304) and low alloy steel (AISI 4140) is described. The emphasis is made on the influence of rotational speed on the microstructure and mechanical properties such as hardness, tensile strength, notch tensile strength and impact toughness of the dissimilar joints. Hardness profiles across the weld show the interface is harder than the respective parent metals. In general, maximum peak hardness is observed on the stainless steel side, while other peak hardness is on the low alloy steel side. A trough in hardness distribution in between the peaks is located on the low alloy steel side. Peak hardness on the stainless steel and low alloy steel side close to the interface increases with a decrease in rotational speed. All transverse tensile joints fractured on stainless steel side near the interface. Notch tensile strength and impact toughness increase with increase in rotational speed up to 1500 r/min and decrease thereafter. The mechanism of influence of rotational speed for the observed trends is discussed in the torque, displacement characteristics, heat generation, microstructure, fractography and mechanical properties.
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  Grain Refinement in a Low Carbon Steel Through Multidirectional Forging

  V Soleymani,B Eghbali

  中国钢铁期刊网. 2012, 19(10): 74-78.

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  Grain refinement is one of the successful and low-cost methods to develop metals having excellent combination of strength and ductility. Low carbon steel was deformed by using multidirectional forging (MDF) technique at room temperature. The influence of strain amount and annealing process on the microstructure and mechanical properties of investigated steel was studied. The grain refinement mechanism was studied by the microstructure observation. The results showed that the grain refinement was attained by multidirectional forging technique. The initial coarser grains of average 38 μm size fragmented into very fine ferrite with grain sizes of about 1.2 μm. After MDF, the strength properties improved significantly, although uniform elongation and elongation decreased with increasing strain.