Growth Kinetics of Laves Phase and Its Effect on Creep Rupture Behavior in 9Cr Heat Resistant Steel

Zhi-xin XIA,Chuan-yang WANG,Chen LEI,Yun-ting LAI,Yan-fen ZHAO,Lu ZHANG

钢铁研究学报(英文版) ›› 2016, Vol. 23 ›› Issue (7) : 685-691.

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钢铁研究学报(英文版) ›› 2016, Vol. 23 ›› Issue (7) : 685-691.
Material

Growth Kinetics of Laves Phase and Its Effect on Creep Rupture Behavior in 9Cr Heat Resistant Steel

  • Zhi-xin XIA1,Chuan-yang WANG2,Chen LEI3,Yun-ting LAI4,Yan-fen ZHAO4,Lu ZHANG4
作者信息 +

Growth Kinetics of Laves Phase and Its Effect on Creep Rupture Behavior in 9Cr Heat Resistant Steel

  • Zhi-xin XIA1,Chuan-yang WANG2,Chen LEI3,Yun-ting LAI4,Yan-fen ZHAO4,Lu ZHANG4
Author information +
文章历史 +

摘要

The effects of Laves phase formation and growth on creep rupture behaviors of P92 steel at 883 K were studied. The microstructural evolution was characterized using scanning electron microscopy and transmission electron microscopy. Kinetic modeling was carried out using the software DICTRA. The results indicated Fe2(W,Mo) Laves phase has formed during creep with 200 MPa applied stress at 883 K for 243 h. The experimental results showed a good agreement with thermodynamic calculations. The plastic deformation of laths is the main reason of creep rupture under the applied stress beyond 160 MPa, whereas, creep voids initiated by coarser Laves phase play an effective role in creep rupture under the applied stress lower than 160 MPa. Laves phase particles with the mean size of 243 nm lead to the change of creep rupture feature. Microstructures at the vicinity of fracture surface, the gage portion and the threaded ends of creep rupture specimens were also observed, indicating that creep tensile stress enhances the coarsening of Laves phase.

Abstract

The effects of Laves phase formation and growth on creep rupture behaviors of P92 steel at 883 K were studied. The microstructural evolution was characterized using scanning electron microscopy and transmission electron microscopy. Kinetic modeling was carried out using the software DICTRA. The results indicated Fe2(W,Mo) Laves phase has formed during creep with 200 MPa applied stress at 883 K for 243 h. The experimental results showed a good agreement with thermodynamic calculations. The plastic deformation of laths is the main reason of creep rupture under the applied stress beyond 160 MPa, whereas, creep voids initiated by coarser Laves phase play an effective role in creep rupture under the applied stress lower than 160 MPa. Laves phase particles with the mean size of 243 nm lead to the change of creep rupture feature. Microstructures at the vicinity of fracture surface, the gage portion and the threaded ends of creep rupture specimens were also observed, indicating that creep tensile stress enhances the coarsening of Laves phase.

关键词

Heat resistant steels / Laves phase / Microstructure / Plastic deformation / Creep rupture

Key words

Heat resistant steels / Laves phase / Microstructure / Plastic deformation / Creep rupture

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夏志新. Growth Kinetics of Laves Phase and Its Effect on Creep Rupture Behavior in 9Cr Heat Resistant Steel[J]. 钢铁研究学报(英文版), 2016, 23(7): 685-691
YAN Zhi-Xin. Growth Kinetics of Laves Phase and Its Effect on Creep Rupture Behavior in 9Cr Heat Resistant Steel[J]. Journal of Iron and Steel Research International, 2016, 23(7): 685-691

参考文献

[1] P.J. Ennis, A. Zielinska-Lipec, O. Wachter, A. Czyrska-Filemonowicz, Microstructural stability and creep rupture strength of the martensitic steel. Acta Mater. 45(1997) 4901-4907.
[2] Z. X. Xia, C. Zhang, N.Q. Fan, Y.F. Zhao, F. Xue, S.J. Liu, Improve creep properties of reduced activation steels by controlling precipitation behaviors. Mater. Sci. Eng. 545A(2012) 91-96.
[3] Z. X. Xia, C. Zhang, Z. G. Yang, TaC precipitation behaviors in reduced activation martensitic steels. J. Mater. Sci. 46(2011) 3151-3156.
[4] H. Tanigawa, H. Sakasegawa, N. Hashimoto, R.L. Klueh, M. Ando, M.A. Sokolov, Irradiation effects on precipitation and its impact on the mechanical properties of reduced-activation ferritic/martensitic steels. J. Nucl. Mater. 367(2007) 42-47.
[5] O. Prat, J. Garcia, D. Rojas, C. Carrasco, G. Inden, Investigations on the growth kinetics of Laves phase precipitates in 12% Cr creep-resistant steels: Experimental and DICTRA calculations. Acta Mater. 58(2010) 6142-6153.
[6] H. Cui, F. Sun, K. Chen, L. Zhang, R. Wan, A. Shan, et al., Precipitation behavior of Laves phase in 10%Cr steel X12CrMoWVNbN10-1-1 during short-term creep exposure. Mater. Sci. Eng. A 527(2010) 7505-7509.
[7] A. Aghajani, F. Richter, C. Somsen, S.G. Fries, I. Steinbach, G. Eggeler, On the formation and growth of Mo-rich Laves phase particles during long-term creep of a 12% chromium tempered martensite ferritic steel. Scr. Mater. 61(2009) 1068-1071.
[8] A. Aghajani, Ch. Somsen, G. Eggeler, On the effect of long-term creep on the microstructure of a 12% chromium tempered martensite ferritic steel. Acta Mater. 57(2009) 5093-5106.
[9] Q. Li, Metall. Precipitation of Fe2W laves phase and modeling of its direct influence on the strength of a 12Cr-2W steel. Mater. Trans. 37(2006) 89-97.
[10] F. Abe, Metall. Effect of fine precipitation and subsequent coarsening of Fe2W laves phase on the creep deformation behavior of tempered martensitic 9Cr-W steels. Mater. Trans. 36(2005) 321-332.
[11] J.S. Lee, H.G. Armaki, K. Maruyama, H. Asahi, Causes of breakdown of creep strength in 9Cr-1.8W-0.5Mo-VNb steel. Mater. Sci. Eng. 428A(2006) 270-275.
[12] K. Yamamoto, Y. Kimura, F. G. Wei, Y. Mishima, Design of Laves phase strengthened ferritic heat resisting steels in the Fe–Cr–Nb(–Ni) system. Mater. Sci. Eng. 329A(2002) 249-254.
[13] V. Knezevic, G. Sauthoff, J. Vilk, G. Inden, A. Schneider, R. Agamennone, et al., Martensitic/Ferritic super heat-resistant 650℃ Steel-design and testing of model Alloys. ISIJ Int. 42(2002) 1505-1514.
[14] G. Dimmlera, P. Weinert, E. Kozeschnik, H. Cerjak, Quantification of the Laves phase in advanced 9-12% Cr steels using a standard SEM. Mater. Character. 51(2003) 341-352.
[15] Y. Tomita, Application of decreased hot-rolling reduction treatments for improved mechanical properties of quenched and highly-tempered low alloy structural steels. J. Mater. Sci. 26(1991)35-42.
[16] J. Cui, I.S. Kim, C. Y. Kang, K. Miyahara, reep Stress Effect on the Precipitation Behavior of Laves Phase in Fe–10%Cr–6%W Alloys. ISIJ Int. 41(2001) 368-371.
[17] L. M. Wang, Z. B. Wang, K. Lu, Grain size effects on the austenitization process in a nanostructured ferritic steel. Acta Mater. 59(2011) 3710-3719.
[18] O. Prat, J. Garcia, D. Rojas, G. Sauthoff, G. Inden, The role of Laves phase on microstructure evolution and creep strength of novel 9%Cr heat resistant steels. Intermetallics 32(2013) 362-372.
[19] K. Maruyama, K. Sawada, J. Koike, Strengthening Mechanisms of Creep Resistant Tempered Martensitic Steel. ISIJ Int. 41 (2001) 641-653.
[20] L. Zhou, G. Liu, X.L. Ma, K. Lu, Strain-induced refinement in a steel with spheroidal cementite subjected to surface mechanical attrition treatment. Acta Mater. 56(2008) 78-87.
[21] M. Tamura, K. Ikeda, H. Esaka, K. Shinozuka, Precipitation Behavior of NbC in 9%Cr1%Mo0.2%VNb Steel ISIJ Int. 41(2001) 908-914.
[22] M. Tamura, T. Iida, H. Kusuyama, K. Shinozuka, H. Esaka, Re-dissolution of VN during Tempering in High Chromium Heat Resistant Martensitic Steel. ISIJ Int. 44 (2004) 153-161.

基金

National Natural Science Foundation of China;National Natural Science Foundation of China;Natural Science Foundation of Jiangsu Province

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