Characterization of inclusions in GCr15 bearing steel by ASPEX and rotary bending fatigue methods
SHI Zhi-yue1, XU Hai-feng1, XU Da1, YU Feng1, WANG Chang2, CAO Wen-quan1
(1. Institute of Special Steels, Central Iron and Steel Research Institute, Beijing 100081, China;
2. Center Laboratory, Central Iron and Steel Research Institute, Beijing 100081, China)
Abstract:In order to explore the best application conditions of those two methods and understand the information of inclusions in bearing steel the ASPEX test and rotating-bending fatigue test of GCr15 bearing steel under vacuum degassing process was investigated. The information of the inclusions including type,shape,size and distribution was analyzed. It was found that using these two methods the inclusion types were found almost same with the spherical inclusions in the GCr15 were rich in Ca,Al and S,and also a small number of sharp TiN inclusions with sharp edges. Using ASPEX for multi-faceted multiple scanning,it was found that the distribution of the maximum size spheroidal B-type alumina inclusions was basically in accord with the result of the rotating-bending fatigue test. According to the test results and the principle of two detection methods,the ASPEX method is more effective for the overall analysis of inclusions in steel,such as inclusion size,shape,type,distribution,etc,meanwhile the application of fatigue method is more advantageous for the detection of large-sized rigid inclusions.
李永德, 杨振国, 李守新, 等.GCr15轴承钢超高周疲劳性能与夹杂物相关性[J]. 金属学报, 2008(08):968-972. (Li Yong-de, Yang Zhen-guo, Li Shou-xin, et al. Correlations between vary high cycle fatigue properties and inclusions of GCr15 bearing steel[J]. Acta Metallurgica Sinica, 2008(08):968-972)[J].金属学报, 2008, 44(8):968-972
[2]
李永德, 杨振国, 李守新, 等.GCr15轴承钢超高周疲劳性能与夹杂物相关性[J]. 金属学报, 2008(08):968-972. (Li Yong-de, Yang Zhen-guo, Li Shou-xin, et al. Correlations between vary high cycle fatigue properties and inclusions of GCr15 bearing steel[J]. Acta Metallurgica Sinica, 2008(08):968-972)[J].金属学报, 2008, 44(8):968-972
[3]
惠卫军, 董瀚, 陈思联.非金属夹杂物和表面状态对高强度弹簧钢疲劳性能的影响[J]. 特殊钢, 1998(06):8-14.(Hui Wei-jun, Dong Han, Chen Si-lian. Influence of non-metallic inclusion and surface condition on fatigue property of high strength spring steel[J]. Special steel, 1998(06):8-14)[J].特殊钢, 1998, (6):8-14
[3]
惠卫军, 董瀚, 陈思联.非金属夹杂物和表面状态对高强度弹簧钢疲劳性能的影响[J]. 特殊钢, 1998(06):8-14.(Hui Wei-jun, Dong Han, Chen Si-lian. Influence of non-metallic inclusion and surface condition on fatigue property of high strength spring steel[J]. Special steel, 1998(06):8-14)[J].特殊钢, 1998, (6):8-14
[4]
马超, 罗海文.扫描电镜和电解萃取法用于超洁净钢中夹杂物的表征[J]. 冶金分析, 2017(08):1-8.(Ma Chao, Luo Hai-wen. Characterization of inclusions in ultra clean steel by SEM and electrolytic extraction[J]. Metallurgical analysis, 2017(08):1-8)[J].冶金分析, 2017, 37(8):1-8
[4]
马超, 罗海文.扫描电镜和电解萃取法用于超洁净钢中夹杂物的表征[J]. 冶金分析, 2017(08):1-8.(Ma Chao, Luo Hai-wen. Characterization of inclusions in ultra clean steel by SEM and electrolytic extraction[J]. Metallurgical analysis, 2017(08):1-8)[J].冶金分析, 2017, 37(8):1-8
[5]
方克明, 王国承.钢中的夹杂物研究从表征到改性[A]: 2006年全国冶金物理化学学术会议, 中国山东济南, 2006[C].(Fang Ke-ming, Wang Guo-cheng. Study of inclusions in steel from characterization to modification[A]. National Symposium on physical and chemical metallurgy of metallurgy in 2006, Ji' nan, Shandong, China, 2006[C])
[5]
方克明, 王国承.钢中的夹杂物研究从表征到改性[A]: 2006年全国冶金物理化学学术会议, 中国山东济南, 2006[C].(Fang Ke-ming, Wang Guo-cheng. Study of inclusions in steel from characterization to modification[A]. National Symposium on physical and chemical metallurgy of metallurgy in 2006, Ji' nan, Shandong, China, 2006[C])
[6]
方克明, 尚德礼, 王存.钢中夹杂物检测及纳米相应用技术前景探索[J]. 鞍钢技术, 2012(02):1-4.(Fang Ke-ming, Shang De-li, Wang Cun, et al. Detection of inclusion in steel and Discuss on application prospect of nano-phase technologies[J]. Angang technology, 2012(02):1-4)[J].鞍钢技术, 2012, (2):1-4
[6]
方克明, 尚德礼, 王存.钢中夹杂物检测及纳米相应用技术前景探索[J]. 鞍钢技术, 2012(02):1-4.(Fang Ke-ming, Shang De-li, Wang Cun, et al. Detection of inclusion in steel and Discuss on application prospect of nano-phase technologies[J]. Angang technology, 2012(02):1-4)[J].鞍钢技术, 2012, (2):1-4
[7]
张立峰, 杨文, 张学伟, 等.钢中夹杂物的系统分析技术[J]. 钢铁, 2014(02):1-8.(Zhang Li-feng, Yang Wen, Zhang Xue-wei, et al. Systematic analysis of non-metallic inclusion in steel[J]. Iron and Steel, 2014(02):1-8)[J].钢铁, 2014, 49(2):1-8
[7]
张立峰, 杨文, 张学伟, 等.钢中夹杂物的系统分析技术[J]. 钢铁, 2014(02):1-8.(Zhang Li-feng, Yang Wen, Zhang Xue-wei, et al. Systematic analysis of non-metallic inclusion in steel[J]. Iron and Steel, 2014(02):1-8)[J].钢铁, 2014, 49(2):1-8
[8]
田超, 刘剑辉, 董瀚.进口与国产轴承钢夹杂物特征的对比研究[J]. 热加工工艺, 2017(24):58-62.(Tian Chao, Liu Jian-hui, Dong Han. Comparative study on inclusion characteristic of imported and domestic bearing steel[J]. Hot working technology, 2017(24):58-62)[J].热加工工艺, 2017, (24):58-62
[8]
田超, 刘剑辉, 董瀚.进口与国产轴承钢夹杂物特征的对比研究[J]. 热加工工艺, 2017(24):58-62.(Tian Chao, Liu Jian-hui, Dong Han. Comparative study on inclusion characteristic of imported and domestic bearing steel[J]. Hot working technology, 2017(24):58-62)[J].热加工工艺, 2017, (24):58-62
[9]
于会香, 邵肖静, 张静, 等.采用ASPEX扫描电镜研究钢中总氧和非金属夹杂物的定量关系[J]. 工程科学学报, 2015(S1):35-44.(Yu Hui-xiang, Shao Xiao-jing, Zhang jing, et al. Study on the qualitative relationship between total oxygen content and non-metallic inclusion in steel with ASPEX SEM[J]. Chinese journal of engineering, 2015(S1):35-44)[J].工程科学学报, 2015, (s1):35-44
[9]
于会香, 邵肖静, 张静, 等.采用ASPEX扫描电镜研究钢中总氧和非金属夹杂物的定量关系[J]. 工程科学学报, 2015(S1):35-44.(Yu Hui-xiang, Shao Xiao-jing, Zhang jing, et al. Study on the qualitative relationship between total oxygen content and non-metallic inclusion in steel with ASPEX SEM[J]. Chinese journal of engineering, 2015(S1):35-44)[J].工程科学学报, 2015, (s1):35-44
[10]
朱苏敏.ASPEX全自动夹杂物分析技术在优化炼钢工艺上的成功应用: 2014年全国炼钢—连铸生产技术会, 中国河北唐山, 2014[C].(Zhu Su-min. ASPEX automated analysis technology for non-metallic inclusion and its successful application in optimizing steel making[A].2014 national steelmaking and Continuous Casting Technology Association, Tangshan, Hebei, China, 2014[C])
[10]
朱苏敏.ASPEX全自动夹杂物分析技术在优化炼钢工艺上的成功应用: 2014年全国炼钢—连铸生产技术会, 中国河北唐山, 2014[C].(Zhu Su-min. ASPEX automated analysis technology for non-metallic inclusion and its successful application in optimizing steel making[A].2014 national steelmaking and Continuous Casting Technology Association, Tangshan, Hebei, China, 2014[C])
[11]
Hansen K T, F?ster S, Natarajan A, et al.Analysis of bearing steel exposed to rolling contact fatigue[J]. Materials Science and Engineering, 2017, 219.[J].Analysis of bearing steel exposed to rolling contact fatigue, 2017, 219(1):-
[11]
Hansen K T, F?ster S, Natarajan A, et al.Analysis of bearing steel exposed to rolling contact fatigue[J]. Materials Science and Engineering, 2017, 219.[J].Analysis of bearing steel exposed to rolling contact fatigue, 2017, 219(1):-
[12]
K SHIOZAWA L L A S.S – Ncurve characteristics and subsurface crack initiation behaviour in ultra-long life fatigue of a high carbon-chromium bearing steel[J]. Fatigue Fract Engng Mater Struct, 2001(24).
[12]
K SHIOZAWA L L A S.S – Ncurve characteristics and subsurface crack initiation behaviour in ultra-long life fatigue of a high carbon-chromium bearing steel[J]. Fatigue Fract Engng Mater Struct, 2001(24).
[13]
马惠霞, 李文竹, 黄磊, 等.轴承钢中硫化物夹杂诱发疲劳裂纹的微观分析[J]. 金属热处理, 2012(03):119-121.(Ma Hui-xia, Li wen-zhu, Huang lei, et al. Analysis of sulphide inclusion induced fatigue crack in bearing steel[J]. Heat treatment of metals, 2012(03):119-121)[J].金属热处理, 2012, 37(3):119-121
[13]
马惠霞, 李文竹, 黄磊, 等.轴承钢中硫化物夹杂诱发疲劳裂纹的微观分析[J]. 金属热处理, 2012(03):119-121.(Ma Hui-xia, Li wen-zhu, Huang lei, et al. Analysis of sulphide inclusion induced fatigue crack in bearing steel[J]. Heat treatment of metals, 2012(03):119-121)[J].金属热处理, 2012, 37(3):119-121
[14]
Ciavarella M, Papangelo A.On the distribution and scatter of fatigue lives obtained by integration of crack growth curves: Does initial crack size distribution matter?[J]. Engineering Fracture Mechanics, 2018, 191:111-124.
[14]
Ciavarella M, Papangelo A.On the distribution and scatter of fatigue lives obtained by integration of crack growth curves: Does initial crack size distribution matter?[J]. Engineering Fracture Mechanics, 2018, 191:111-124.
[15]
Jiang H, Luo T, Li G, et al.Fatigue life assessment of electromagnetic riveted carbon fiber reinforce plastic/aluminum alloy lap joints using Weibull distribution[J]. International Journal of Fatigue, 2017, 105:180-189.
[15]
Jiang H, Luo T, Li G, et al.Fatigue life assessment of electromagnetic riveted carbon fiber reinforce plastic/aluminum alloy lap joints using Weibull distribution[J]. International Journal of Fatigue, 2017, 105:180-189.