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Determination method of variable valence iron in magnetite using electron probe micro-analyzer |
ZHAO Tong-xin 1, CUI Hui-jie 2, HU Xiao-chun 1, SUN You-bao 1, HUANG Tao-hong 1 |
1. Analytical Applications Center, Shanghai Branch, SHIMADZU(CHINA) Co., Ltd., Shanghai 200233, China;
2. Analytical Applications Center, Beijing Branch, SHIMADZU(CHINA) Co., Ltd., Beijing 100020, China |
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Abstract The magnetite sample was determined by all-elements test method through taking good use of advantages of Shimadzu EPMA (electron probe micro-analyzer) in instrument configuration. In other words, all elements in magnetite including ultra-light oxygen was directly determined. Then the contents of variable valence elements were calculated according to the principle of electric neutrality balance. The characteristics of Lβ/Lα of FeO and Fe2O3 contents were verified by state analysis. The testing results were relatively satisfactory.
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Received: 30 October 2019
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