|
|
Test and analysis of needle-like metallographic sample in micro-nano scale |
YANG Xiao1, PAN Hengpei1, WANG Shining1, LI Xuefeng1,2, ZHANG Xinyao1,2, GAO Lingqing1,2 |
1. Luoyang Ship Material Research Institute, Luoyang 471023, China; 2. Henan Key Laboratory of Technology and Application Structural Materials for Ships and Marine Equipments, Luoyang 471023, China |
|
|
Abstract In the process of metallographic analysis, the insetting of needle-like sample in micro-nano scale will easily cause the capillary phenomenon, which leads to the limited resolution of metallographic structure. As a result, it is difficult to accurately evaluate the micro structure. The needle-like sample in micro-nano scale were treated by grinding and polishing, and then eroded with the chemical reagents. After that, the sample was placed in ethanol and acetone solution for ultrasonic treatment followed by drying with a hair dryer. The results showed that due to the low melting point and high volatility of acetone solution, the addition of ultrasonic treatment in acetone solution in the process of conventional micro-nano metallographic sample could effectively remove the residual solution between the mosaic material and the sample. The occurrence of capillary phenomenon was reduced, which could ensure the clear observation of metallographic sample as well as the effective characterization of microstructure.
|
Received: 26 August 2022
|
|
|
|
[1] |
尹立新,郭雁行,刘晓岚. 图像分析仪在金相检验中的应用[J].物理测试,2004,22(2):38.
|
[2] |
刘晓磊,时飞扬,陈昌华,等. 35 MN液压机缸体裂纹检验分析[J].物理测试,2022,40(6):21.
|
[3] |
Alain S, Michel N, Jacques S, et al. Effect of dynamic contact angle on capillary rise phenomena[J]. Colloids and Surfaces A,2000,161:81.
|
[4] |
Lei X, Anna L, Jun H, et al. Wetting and capillary phenomena of water on mica[J]. J Phys Chem B,1998,102:540.
|
[5] |
Brackbill J U, Kothe D B, Zemach C. A continuum method for modeling surface tension[J]. J Comput Phys,1992,100:335.
|
[6] |
Aleksandr V M, Christopher J C, Donald G T. Universal solvation model based on solute electron density and on a continuum model of the solvent defined by the bulk dielectric constant and atomic surface tensions[J]. J Phys Chem B, 2009,113: 6378.
|
[7] |
David R, Neumann A W. Contact angle patterns on low-energy surfaces[J]. Adv Colloid Interface Sci, 2014,206:46.
|
[1] |
YANG Kai. Discussion about the mechanical properties relationship between the natural cooling and 200 ℃ water cooling HRB400E[J]. , 2018, 36(3): 15-20. |
[2] |
ZHANG Yong- jun,ZHANG Peng- cheng,HAN Jing- tao. Cold deformation behavior of graphitized carbon steel[J]. , 2018, 30(10): 796-801. |
[3] |
CAO Zhi-gang, DU Zhong-ze, FANG Yi-yuan, ZHANG Xiao-yuan, WANG Xiao-guo. Cause and analysis of crack and scratches on the surface of sucker rod steel[J]. , 2018, 37(03): 62-66. |
[4] |
GUO Wei-da,MA Zhong-wei,XIAO Qiang,HU Peng,CHEN Yong-sheng,ZHANG Hui. Simulation experiments for slivers on the edge of heavy plate[J]. Chinese Journal of Iron and Steel, 2015, 34(4): 9-12. |
[5] |
SHI Lei, FENG Ding, MA Wei, YAN Jian, LI Zhi-min, ZHANG Hong. Metallographic Analysis of Casing Pipes Based on Development of Offshore Well Completion[J]. Chinese Journal of Iron and Steel, 2014, 32(5): 49-52. |
[6] |
WANG Hai-bao,,ZHANG Jiong-ming,ZHAO Xin-yu,LIU Yang,WANG Wen-jun,ZHEN Xin-gang. Effect of Cooling Pattern on Surface Microstructure of Slab[J]. Iron and Steel, 2013, 48(4): 35-39. |
|
|
|
|