Simulation and experiment investigations on fabrication of Fe-based amorphous powders by a novel atomization process equipped with assisted gas nozzles

Jia-qi Liu, Yan-nan Dong, Pu Wang, Huan Zhao, Jing Pang, Xiao-yu Li, Jia-quan Zhang

钢铁研究学报(英文版) ›› 2023, Vol. 30 ›› Issue (6) : 1142-1155.

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钢铁研究学报(英文版) ›› 2023, Vol. 30 ›› Issue (6) : 1142-1155. DOI: 10.1007/s42243-022-00855-8
论著

Simulation and experiment investigations on fabrication of Fe-based amorphous powders by a novel atomization process equipped with assisted gas nozzles

  • Jia-qi Liu1, Yan-nan Dong1, Pu Wang1, Huan Zhao2, Jing Pang2, Xiao-yu Li2, Jia-quan Zhang1
作者信息 +

Simulation and experiment investigations on fabrication of Fe-based amorphous powders by a novel atomization process equipped with assisted gas nozzles

  • Jia-qi Liu1, Yan-nan Dong1, Pu Wang1, Huan Zhao2, Jing Pang2, Xiao-yu Li2, Jia-quan Zhang1
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摘要

Based on computational fluid dynamics method, the effect of atomization gas pressure on the atomization efficiency of Laval nozzle was studied, and then a discrete phase model was established and combined with industrial trials to study the effect of a new type of assisted gas nozzles (AGNs) on powder size distribution and amorphous powder yield. The results show that increasing the atomization pressure can effectively improve the gas velocity for the Laval nozzle; however, it will decrease the aspiration pressure, and the optimal atomization pressure is 2.0 MPa. Compared with this, after the application of AGNs with the inlet velocity of 200 m s-1, assisted gas jet can increase the velocity of overall droplets in the break-up and solidification area by 40 m s-1 and the maximum cooling rate is increased from 1.9×104 to 2.3 ×104 K s-1. The predicted particle behavior is demonstrated by the industrial trails, that is, after the application of AGNs, the median diameter of powders d50 is decreased from 28.42 to 25.56 lm, the sphericity is increased from 0.874 to 0.927, the fraction of amorphous powders is increased from 90.4% to 99.4%, and only the coercivity is increased slightly due to the accumulation of internal stress. It is illustrated that the AGNs can improve the yield of fine amorphous powders, which is beneficial to providing high-performance raw powders for additive manufacturing technology.

Abstract

Based on computational fluid dynamics method, the effect of atomization gas pressure on the atomization efficiency of Laval nozzle was studied, and then a discrete phase model was established and combined with industrial trials to study the effect of a new type of assisted gas nozzles (AGNs) on powder size distribution and amorphous powder yield. The results show that increasing the atomization pressure can effectively improve the gas velocity for the Laval nozzle; however, it will decrease the aspiration pressure, and the optimal atomization pressure is 2.0 MPa. Compared with this, after the application of AGNs with the inlet velocity of 200 m s-1, assisted gas jet can increase the velocity of overall droplets in the break-up and solidification area by 40 m s-1 and the maximum cooling rate is increased from 1.9×104 to 2.3 ×104 K s-1. The predicted particle behavior is demonstrated by the industrial trails, that is, after the application of AGNs, the median diameter of powders d50 is decreased from 28.42 to 25.56 lm, the sphericity is increased from 0.874 to 0.927, the fraction of amorphous powders is increased from 90.4% to 99.4%, and only the coercivity is increased slightly due to the accumulation of internal stress. It is illustrated that the AGNs can improve the yield of fine amorphous powders, which is beneficial to providing high-performance raw powders for additive manufacturing technology.

关键词

Computational fluid dynamics / Discrete phase model / Assisted gas nozzle / Amorphous powder / Atomization

Key words

Computational fluid dynamics / Atomization / Amorphous powder / Assisted gas nozzle / Discrete phase model

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Pu Wang, Jia-qi Liu, Yan-nan Dong, . Simulation and experiment investigations on fabrication of Fe-based amorphous powders by a novel atomization process equipped with assisted gas nozzles[J]. 钢铁研究学报(英文版), 2023, 30(6): 1142-1155 https://doi.org/10.1007/s42243-022-00855-8
Pu Wang, Jia-qi Liu, Yan-nan Dong, et al. Simulation and experiment investigations on fabrication of Fe-based amorphous powders by a novel atomization process equipped with assisted gas nozzles[J]. Journal of Iron and Steel Research International, 2023, 30(6): 1142-1155 https://doi.org/10.1007/s42243-022-00855-8

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