15 October 2025, Volume 43 Issue 5
    

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    Test and Research
  • ZHANG Zhaogang
    Physics Examination and Testing. 2025, 43(5): 1-7. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240090
    Abstract ( ) Download PDF ( )   Knowledge map   Save
    The aluminum shell of lithium-ion battery plays the roles of sealing and protection for the positive and negative electrodes, separator, and electrolyte inside the package. Its defects could affect the safety, sealing property, and energy utilization efficiency of the battery. In this study, 53148115-type 3003-H14 aluminum alloy shells were employed to systematically investigate the effects of wall thickness, defect and corrosive environment on the property of tensile, pressure resistance and corrosion. The results showed that the shells with wall thickness of 1.0 mm could satisfy the strength requirements of lithium-ion battery. The location of defects had an important influence on the sealing property. The arc radius depression at the corners of aluminum shell has almost no effect on the blasting pressure, while large depressions or damages on the surface significantly reduce the pressure resistance strength. The crystal structure had no change after exposure to water and 5 g/L NaCl solution for 24 h. However, the surface roughness increased with the corrosion time. NaOH solutions caused pronounced surface corrosion, and new reaction substances were formed within 0.5 min in 50 g/L NaOH solution, accompanied by pitting and powdering.
  • Measuring Technology
  • HONG Gang, QIU Jiayan, JIANG De, ZHAO Han, JIA Yanqing LI Siyuan, SHI Huachao, YU Bo
    Physics Examination and Testing. 2025, 43(5): 8-16. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250037
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    The measurement resolution of impact fracture image analyzer is limited by the optical lens, which cannot meet the requirements of metrological characteristics regarding display resolution. In order to improve the display resolution of impact fracture images, the super resolution fracture image analysis was investigated to solve the problem of low resolution of impact fracture images. The original resolution about 0.03 mm was increased to about 0.003 7 mm, which could meet the requirements of relevant standards. In order to meet both the requirements of impact fracture morphology analysis and the display resolution requirements for metrological calibration characteristics, the tower decomposition amplification enhancement method was adopted in this study. Two different types of impact fractures were photographed on the impact fracture image analyzer to obtain the original fracture images, and then the fracture images were subjected to 8 times tower decomposition amplification processing. Through the algorithm evaluation, it was found that the enlarged fracture image maintained good similarity and information content with the original image, which conformed to the measurement principles of geometric quantities. Finally, an uncertainty evaluation was conducted and the results were provided.
  • CHEN Jile, LI Jiawei, DU Yanling, WU Weiying, HUANG Guangle, CHEN Jianfeng
    Physics Examination and Testing. 2025, 43(5): 17-22. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240087
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    The detection of cracks in natural gas pipelines is a critical link for ensuring the safety of energy transmission, wherein the influence of coating thickness on the efficacy of array eddy current testing directly affects the inspection reliability. Three types of crack depth (i.e.,0.2, 0.3, and 0.4 mm) in the heat-affected zone of natural gas pipeline welds were systematically investigated by array eddy current technology. The effect of coating thickness ranging from 0 to 0.6 mm on the detection signals was quantitatively analyzed. The experimental results demonstrated a significant negative correlation between coating thickness and crack detectability. For the cracks with depth of 0.2 mm, the signal-to-noise ratio (SNR) decreased to an undetectable level at 0.1 mm coating thickness. For the cracks with depth of 0.3 mm, the SNR remained 1.8 when the coating thickness was 0.4 mm, while it decreased to 1.4 when the coating thickness was 0.5 mm. For the cracks with depth of 0.4 mm, the SNR was 1.4 when the coating thickness was 0.6 mm. The research discussed the critical detectable coating thickness for cracks with various depths, and it provided experimental evidence for selecting the engineering inspection parameters.
  • WANG Liang, MA Chenchen, QIU Junxin, CHENG Chong
    Physics Examination and Testing. 2025, 43(5): 23-31. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240079
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    Manual conventional ultrasonic testing might fail to detect the non-metallic inclusion defects in planetary gears of wind turbine gearboxes. In order to reduce the failure probability caused by the defects, an automatic phased array ultrasonic testing method was developed to replace the conventional manual ultrasonic testing for detection of defects in planetary gears of wind turbine gearboxes. Starting from the design and manufacturing of equipment, the following contents, such as the design of reference test block and wedge block, the setting of electronic linear scanning process parameters before detection, as well as the process verification methods, were discussed in this paper. The experiments showed that the internal defects in planetary gears of wind turbine gearboxes could be successfully detected using automatic phased array ultrasonic testing equipment combining with the designed parameters of wedge, probe, and process. It indicated that the proposed method was effective and reliable for detection of internal defects in planetary gears of wind turbine gearboxes.
  • QIAN Jiang, ZHANG Yuan, HAN Qingsheng, SUN Yuhan, JIANG Dongqin
    Physics Examination and Testing. 2025, 43(5): 32-37. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250004
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    Bar materials,as important raw materials for key components such as bearings and chains, their quality directly affects the safety performance of the downstream products. For rods with a diameter not exceeding 50 mm, the magnetic flux leakage non-destructive testing technology is commonly used for defect detection, but it has the disadvantages of high loss and high cost. The application of infrared thermal imaging detection technology in detection of surface defects of small-size bars was investigated. This technology heats the surface of small-size bars in motion by controlling a high-frequency eddy current heat source. The surface temperature field information was collected with infrared camera, and analyzed through image processing technology. The characteristic information of surface defects was obtained by the temperature change rate. The test results showed that when the ratio of defect depth to surface roughness of the bars was greater than 3 ∶1, this detection method could accurately distinguish the defect range from the image. When the motion speed was within the range of 0.5 to 1.5 m/s and the depth of the artificial damage grooves was within the range of 0.1 to 1.1 mm, the defect detection rate was greater than 99.5% and the false alarm rate was less than 0.5%. The feature extraction technology could precisely calculate and obtain the geometric shape features (length, width, etc. of key parameters) and spatial position information of defects. The deviation in the length direction was within ±3 mm and the deviation in the angle direction was within ±5°.
  • HAO Weikang, HUANG Hao, CHEN Jia, ZHANG Yang, GUO Hongze, QU Xinxin
    Physics Examination and Testing. 2025, 43(5): 38-42. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250095
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    The application effect of high-frame-rate narrow-array detector in non-destructive testing of pipeline welds was investigated. The influence of different detection parameters on image quality was analyzed in detail, including encoding factor, exposure dose, frame rate, and scanning speed. Through a series of experiments, the specific effects of these parameters on the imaging sensitivity, including system resolution, signal-to-noise ratio (SNR), and grayscale values, were evaluated. The experimental results showed that reasonable selection of encoding factors and exposure dose could significantly improve the image clarity and optimize the imaging quality, thus effectively enhancing the detection accuracy of weld defects. However, excessively high frame rate sand scanning speed may lead to a decrease in image uniformity and SNR, thereby affecting the detection effect. The further experiments have verified the crucial role of parameter calibration in imaging quality optimization, which provided reliable scientific basis and experimental data support for weld detection. The optimization of detection parameters not only helped to improve the image quality, but also significantly enhanced the detection accuracy of weld defects, thereby promoting the widespread application and development of high-frame-rate narrow-array detector technology in non-destructive testing of pipeline welds.
  • SHEN Haihong, KANG Lihong, WAN Ce, JIANG Mingming, LIU Yujie, YAO Yifei
    Physics Examination and Testing. 2025, 43(5): 43-48. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240109
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    The thickness measurement by ultrasonic has been widely used in industrial fields. In this study, the principle and method of thickness measurement by ultrasonic were elaborated based on one practical application case. The solutions for abnormal problems in measurement of steel pipe thickness by ultrasonic thickness gauge were further discussed. The abnormality of measured values was possibly caused by the material thinning or the defects inside the materials. A-scan pulse reflection ultrasonic flaw detector should be used to assist in the measurement of ultrasonic thickness method. The background noise of A-scan pulse reflection ultrasonic flaw detector was adjusted to 10% of full screen for the scanning at the thickness measurement point. If no reflected wave significantly higher than the noise level was detected before the bottom wavefront, it indicated that there were no defects affecting the thickness measurement along the path traversed by the sound velocity of ultrasonic thickness gauge. In this case, the measured value was calculated based on the reflection time of bottom wave at the measured location, and this value was consistent with the actual thickness at the measured point. For the condition that there were reflected waves significantly higher than the noise level before the bottom wavefront, if the amplitude of the reflected signal exceeded the requirements specified in the standards, the material failed the flaw detection, and the measurement of thickness was not further required according to material flaw detection standards. If the amplitude of the reflected signal did not exceed the requirements specified in the standards, the material passed the flaw detection. While, it should be noted that the measured value at this time was not calculated based on the reflection time of bottom wave at the measured location. Instead, it was a smaller value caused by the reflected waves from defects that were allowed to exist in the material. In such cases, an ultrasonic flaw detector should be used to read the material thickness at that point based on the position of bottom wave. It was recommended that in national product standards, when the specified material thickness measurement methods were ruler measurement and ultrasonic measurement, if there was a discrepancy between the two above, it should be clearly stated that the ruler measurement result shall prevail, so as to avoid disputes in engineering.
  • Defect Analysis
  • SUN Jiangbo, PING Yu, REN Shuai, ZHANG Hongqi
    Physics Examination and Testing. 2025, 43(5): 49-53. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240097
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    Through analogue simulation, metallographic structure analysis, high-temperature thermoplastic test and fracture morphology analysis of edge crack defects in Q460C angle steel, the formation mechanism of these defects was explored. The results showed that there were oxidation material spots, decarburization and ferrite grain growth in the defective parts of edge cracks in angle steel. The edge cracks in angle steel were caused by the inheritance of cracks in the inner arc angles of casting billet. Q460C continuous casting billet had obvious high-temperature plastic zone and low-temperature brittle zone. The high-temperature plastic zone was in range of 975-1 350 ℃, and the low-temperature brittle zone was in range of 600-950 ℃. When the temperature increased from 950 ℃ to 975 ℃, the section shrinkage rate increased from 34% to 85%. On this basis, the process optimization measures, such as improving the purity of molten steel, stabilizing the drawing speed, controlling the superheat of the middle ladle, adjusting the specific water volume of the secondary cooling, and increasing the temperature before straightening of the continuous casting billet, were proposed for the problem of crack defects at the edge of Q460C angle steel. Then the surface quality at angle of casting billet was significantly improved, and the crack defects on the surface of angle steel were fully controlled.
  • LI Xiaoyan, CHEN Honghe, HAN Shudong, ZHAI Youyou, HU Ming
    Physics Examination and Testing. 2025, 43(5): 54-59. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240091
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    The spring steel is a specialized type of steel used for manufacturing mechanical springs and saw blades. It has high elastic limit, excellent fatigue resistance, good toughness and plasticity, which enables it to withstand significant deformation without fracture. During the wire drawing process of 65Mn spring steel wire rod produced by one factory used in vehicle, the fracture incidents occurred. At the fracture location of the wire rod samples, fractured samples were cut for analysis at approximately 100 mm from the fracture site with a hydraulic sampling shear to find out the causes and provide some suggestions to solve this problem. The fractured samples during wire drawing were analyzed by scanning electron microscopy (SEM), optical emission spectrometry (OES), optical microscopy (OM), and digital microhardness tester. The macro-fractography, micro-fractography, chemical composition testing, and metallographic examination were conducted for the fractured site. The microhardness test was performed for the abnormal microstructures. The comprehensive analyses above revealed that the primary cause of fracture during sample drawing was related to the surface damage and the formation of deformation-induced martensite in the structure of wire rod. The reasons for the formation of deformation-induced martensite were discussed, and the technical measures to prevent its occurrence were proposed.
  • ZHAO Xuyan, CHENG Yuan, WENG Quanrong, SHI Feiyang
    Physics Examination and Testing. 2025, 43(5): 60-65. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240080
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    After heat treatment of 30CrMo valve cover produced by one forging factory, some cracks were observed at the interface between the surface and the through hole of during the finish machining stage. The valve covers with crack defects were sampled by dissection and analyzed by macroscopic inspection, metallographic inspection, and scanning electron microscopy inspection to find out the causes of cracking. The results indicated that the surface cracks at the through hole of valve cover belonged to quenching cracks, which were originated from the corner position between the through hole and the upper surface. The further analysis showed that the interface between the upper surface of valve cover and the through hole was roughly machined into a right-angle structure before heat treatment. This geometric feature became a stress concentration source for quenching crack initiation during the heat treatment process due to the synergistic effect of structure stress and thermal stress. This study clarified the property and formation mechanism of cracks, providing a theoretical basis for the optimization of valve cover processing. It was recommended to improve the corner transition structure or adjust the heat treatment process parameters to reduce stress concentration degree and avoid the occurrence of quenching crack defects.
  • ZENG Jiaqi, WANG Baoliang, LI Zewei, XU Hong, SONG Jianhua, ZHOU Haiyan
    Physics Examination and Testing. 2025, 43(5): 66-69. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240084
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    Through the penetrant inspection of one fixed bed reactor, it was found that there were many tiny cracks in the heat-affected zone of dissimilar steel welding head circumferential weld. The length of cracks was 1-1.5 mm with no bifurcation, and the crack direction was perpendicular to the weld. The surface cracks were analyzed by means of spectrum detection, hardness detection, alternating current electromagnetic field detection and metallographic detection. The results showed that the welding process was unreasonable, because the multi-layer and single-pass welding method generally required a large linear energy, which made the austenitic stainless-steel stay at the sensitization temperature (450-850 ℃) for an excessively long time, resulting in the precipitation of chromium carbide from the grain boundary. As a result, the chromium-poor areas were formed and the material was sensitized. Therefore, the grains were coarser, and the bonding force between grains was further weakened. In addition, the welding of dissimilar steels also caused large welding residual stress in the later cooling process of austenitic stainless steel. Moreover, due to the particularity of austenitic stainless steel, the post-weld heat treatment was generally not carried out, which made this part of residual stress preserved. Under the comprehensive action of the above reasons, some micro-cracks were produced. In view of the above problems, some improvement suggestions were put forward from the aspects of design, manufacture and use.
  • GONG Bitao, YANG Lianghui, XIAO Yang, ZHANG Zheng, YANG Jiadian, WU Yongan
    Physics Examination and Testing. 2025, 43(5): 70-74. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240071
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    After finish machining of 1.4462 alloy forgings, some densely distributed defects suspected to be "holes" on the part surface were observed in fluorescence inspection, and these defects were in a locally dense distribution state. Such defects would reduce the mechanical properties, corrosion resistance, and service life of the parts, thus affecting the precision and surface quality of finish machining. During use, these defects could cause sudden fracture or failure of the parts, leading to safety accidents. Therefore, it was particularly important to avoid the occurrence of forging defects. In order to explore the causes of the “hole” defects, the defect characteristics were observed through scanning electron microscope (SEM), and it was concluded that they might belong to inclusion defect. For typical defects, further scanning electron microscope inspection and energy spectrum (EDS) analysis were conducted to determine that the defect characteristics belong to typical inclusion defects. There was a significant difference in the elemental composition between the defect interior and the matrix. The content of aluminum and oxygen elements in the defect interior was significantly higher than that of the matrix. Therefore, this type of defect could be identified as a brittle oxide defect. The generation of brittle oxides mainly occurred during the deoxidation stage of electric furnace steelmaking, which could be improved by increasing the deoxidation time during steelmaking or multiple smelting processes. Meanwhile, the material should be inspected by flaw detection after formation and lathing so that to find and remove the defects in time.
  • Subject Discussion
  • YU Zhengguang, JIANG Lei, YANG Jihui, ZHANG Xiaolin, CAO Hai
    Physics Examination and Testing. 2025, 43(5): 75-79. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240093
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    A high-temperature creep testing system including series of testing instruments and heterogeneous data within the supporting environment subsystems was integrated based on the data warehouse technology. A laboratorysystem integration framework and heterogeneous data processing procedures for various data sources have been established. The laboratory data server and Mysql+Redis database were set up and configured. The software program for extracting, transforming and transmitting of data was developed and designed. The results showed that the centralized acquisition, processing, storing and share of testing data, running state and environmental data of high-temperature creep equipment could be realized. By means of B/S structure server and token classifying security policy, the remote real-time detection and chart data analysis for application of multi-user, cross platform and hierarchical level were realized. Meanwhile, it also provided the data access interface.