15 February 2026, Volume 44 Issue 1
    

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    Test and Research
  • SUN Changzheng, XU Lixiong, LIU Huimei, XIONG Junwei, HU Haijiang, XU Guang
    Physics Examination and Testing. 2026, 44(1): 1-7. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240104
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    Decarburization often occurs in steel during heat treatment, causing changes in the composition of the surface layer matrix. It directly affects the surface layer phase transformation behavior and microstructure, thus impacting mechanical properties, particularly microhardness. Therefore, it is essential to clarify the influence law of heat treatment decarburization on the surface microstructure evolution and microhardness distribution of medium carbon alloy steel. Thus, the decarburization behavior of medium carbon alloy steel (Fe-0.43C-1.90Si-2.83Mn-0.57Al-0.057Cu) during heating and austenitization was investigated. The influence law of decarburization on the phase transformation, microstructure and microhardness of the steel surface layer was discussed by means of scanning electron microscope(SEM), electron probe analyzer(EPMA) and other methods, combined with heat treatment process of different isothermal temperatures of 630~690 ℃and quenching conditions. The results showed that heating decarburization and isothermal treatment significantly affected the surface phase transformation and microstructure morphology. When the isothermal temperature was 670 ℃ and above, the outer layer microstructure was mainly equiaxed ferrite arranged neatly. When the isothermal temperature was 650 ℃ and below, the decarburized layer microstructure showed columnar ferrite and martensite arranged alternately. When isothermal transformation was carried out at 630 ℃ and then followed by quenching, pearlite matrix microstructure could be obtained, and martensite would form between pearlite and ferrite. This was quite different from ferrite single-phase or two-phase decarburized layer microstructure reported in previous literature. The formation mechanism of the interlayer martensite microstructure was analyzed in combination with the diffusion of alloying elements and phase transformation. The results could provide a basis for the decarburization and heat treatment process of medium carbon alloy steel.
  • LI Xin, ZHANG Long, MA Zichao, GAO Lei, YIN Limeng
    Physics Examination and Testing. 2026, 44(1): 8-14. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250098
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    The connection quality between copper and tin interfaces directly affects the reliability of electronic devices. There are significant differences in their physical and chemical properties, and traditional welding methods are difficult to form stable joints.Based on the establishment of flyer plate dynamics model for copper/tin heterogeneous metal electromagnetic pulse welding (EMPW), the collision process and the stress distribution law at the interface of welding under different gasket spacings (20-40 mm) and collision speeds (200-500 m/s) were investigated in this paper, providing theoretical support for the optimization of the copper/tin EMPW process. The flyer plate dynamics simulation results indicated that increasing the gasket spacing significantly alleviated stress concentration in the welding zone. When the gasket spacings increased from 20 mm to 40 mm, the stress in the copper welding zone decreased from 171.43 MPa to 161.64 MPa, and that in the tin welding zone decreased from 37.26 MPa to 26.21 MPa. On the other hand, increasing the collision speed markedly intensified the stress in the welding zone. As the collision speed rised from 200 m/s to 500 m/s, the stress in the copper welding zone increased from 122.56 MPa to 181.10 MPa, and that in the tin welding zone increased from 33.91 MPa to 55.15 MPa. In addition, scanning electron microscope (SEM) was used to characterize the interfacial morphology of copper/tin welded joints under discharge energies ranging from 12 kJ to 30 kJ. With the increase of discharge energy, the joint interface evolved from a flat morphology to a wavy structure, and finally formed a hook-like morphology.
  • HONG Bing, BI Wenya, ZHANG Xiaozhao, LI Runman ZHENG Liling, ZHANG Pu, LIU Shizhe, ZHOU Fengluan
    Physics Examination and Testing. 2026, 44(1): 15-21. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250080
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    It is of great significance for optimizing its heat treatment process under high-temperature service conditions to investigate the effects of different heat treatment processes on the microstructure properties of GH4169 alloy. The performance differences of GH4169 alloy under different heat treatment conditions were investigated systematically by combining mechanical properties with microstructure analysis. The results indicated that after a solution treatment at (975±10) ℃ for 1 h, followed by aging treatment at (720±10) ℃ for 8 h, and furnace cooling to (620±10)℃ at (50±10)℃/s with an 8 h hold, and then air cooling aging treatment(referred to as Process 1), the microstructure of GH4169 alloy sample had transformed from austenite to austenite and carbides. Based on Process 1, secondary aging was carried out at 680 ℃ for 500 h with air cooling, and at 730 ℃ for 500 h with air cooling (referred to as Process 2 and 3). It was found that the microstructure of the samples transformed into austenite, δ phase, and carbides. The GH4169 alloy samples processed by Process 1 exhibited the best comprehensive mechanical properties. Their tensile strength at room temperature and 650 ℃, as well as their high-temperature endurance life and low-cycle fatigue performance, were all superior to those of Processes 2 and 3. Process 3 resulted in a significant decrease in mechanical properties due to the extensive transformation of γ″ phases into coarse lamellar δ phases during 730 ℃ long-term aging.
  • YU Haiyan, HU Congqing, CHEN Fanhu, GUO Ailin, CAO Xinming
    Physics Examination and Testing. 2026, 44(1): 22-27. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240102
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    It is of great significance to investigate the influence of solution heat treatment and aging hardening on the carbide precipitation in TP304H austenitic stainless steel for understanding the performance variation laws and extending the service life of the material. TP304H austenitic stainless steel samples were subjected to solution heat treatment under different cooling conditions and aging hardening for different durations. The samples were observed with metallographic microscope, and the intergranular corrosion test was conducted according to the ASTM A262-2015 (2021) standard E method. The precipitation morphology, distribution and composition change laws of carbides were analyzed under different cooling conditions of solution heat treatment and different aging hardening times. The results showed that good microstructures were both obtained by direct water quenching and air cooling for 2 minutes followed by water quenching. A slower cooling method resulted in the precipitation of carbides at the grain boundaries, and even a slower cooling rate led to the presence of harmful phases, indicating that the cooling method and cooling degree had a significant impact on the carbide precipitation in TP304H austenitic stainless steel. The longer the aging hardening time, the more severe the carbide precipitation and harmful phases, thereby affecting the microstructure and corrosion resistance of the material. When the aging hardening time was 1 h, the intergranular corrosion E method test failed, indicating that the corrosion resistance of the sample had significantly declined. Therefore, when TP304H austenitic stainless steel is used in high-temperature environment, it is necessary to consider the influence of high-temperature conditions on microstructure and properties of the material.
  • Measuring Technology
  • YANG Dongping, GAO Shasha, LI Wei, SHI Shuang, YUAN Xin’an WANG Zhanpeng, LIU Guangxu, BI Zhuanglong
    Physics Examination and Testing. 2026, 44(1): 28-37. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240107
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    Aluminum and its alloys are widely used in aerospace and other fields due to their light weight, high strength, and corrosion resistance and other characteristics. However, their structures are susceptible to localized corrosion and fatigue cracking, leading to the propagation of surface and subsurface cracks that threaten safety. Based on the defect detection technology of the phase advance characteristic of multi-frequency alternating current field measurement(ACFM), this paper established a theoretical model of the phase advance characteristic. Combined with COMSOL finite element simulation and experimental verification, a detection system containing tunnel magnetoresistance (TMR) sensor, lock-in amplifier and LabVIEW processing program was built. The precise classification and depth quantification of 6 groups of surface cracks with a depth of 4 to 9 mm and 6 groups of subsurface cracks with a depth of 1 to 6 mm were discussed. The results demonstrated that the magnetic field signal along z-direction (Bz) for surface cracks consistently exhibited a "trough-peak" pattern. In contrast, the Bz signal direction for subsurface cracks reversed under high-frequency excitation, and this phase characteristic enabled effective differentiation between the two crack types. Furthermore, a transition signal lacking peaks or troughs, induced by the offset frequency, occurred near the burial depth of subsurface cracks. A linear relationship existed between this offset frequency and the burial depth. The maximum relative error recorded experimentally was only 1.122%, confirming the reliability of the burial depth assessment. This technique provides a novel approach for the high-precision detection and quantification of hidden cracks in aluminum structures.
  • ZHENG Renren, XIE Jinli, SHI Songyi, XIE Mingzhao, SUN Zhimin, QIN Hailong
    Physics Examination and Testing. 2026, 44(1): 38-46. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250001
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    Superalloy ring components are crucial load-bearing components in aerospace, and residual stress is one of the key factors influencing their processing deformation and service life. Contour method enables comprehensive characterization of internal residual stress distribution, providing core data support for stress regulation, deformation mitigation, and service reliability improvement. This study focused on such superalloy ring components, employing contour method to investigate their residual stress evolution before and after heat treatment. To address the low efficiency of contact coordinate measuring machine (CMM) in contour method testing, the influence of non-contact optical scanning (NCOS) on residual stress testing of superalloy ring components by contour method testing was explored. The results showed that the residual stress of initial state sample was distributed in an outward tensile and inward compressive pattern. The maximum tensile stress was 658 MPa and the maximum compressive stress was 247 MPa, with a relatively large stress gradient. During heat treatment, residual stress evolved in two stages. During the heating stage, the initial stress gradually released as the material strength decreased. During the cooling stage, due to the difference in cooling rates at the edges and the core, an external pressure and internal tension distribution was formed. The maximum tensile stress dropped to 76 MPa, and the compressive stress was 204 MPa. The stress values and gradients had significantly decreased. NCOS and CMM yielded consistent stress distribution patterns, but the test values of NCOS were affected by the stress gradient. When the stress gradient was large, the measured value was smaller; when the stress gradient was small, the measured value was larger. This study clarified the residual stress evolution law of such components, providing a basis for heat treatment process optimization, and verified that NCOS was suitable for residual stress testing of superalloy ring components, with attention to the impact of NCOS data smoothing on test results.
  • WU Hong, SU Dashuai, ZOU Yulin
    Physics Examination and Testing. 2026, 44(1): 47-53. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240096
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    To ensure the quality and the use safety of fastener hole, the analysis and research on its eddy current testing signals have received extensive attention. The influence of aperture gap on rotating eddy current testing signal was discussed, aiming to achieve the goal of detecting fasteners holes with a larger range of aperture diameters with fewer probes. Using Ti-6Al-4V titanium alloy and 4340 steel as representative materials, rigid rotating eddy current probes with nominal diameters of ø4.76 mm, ø6.35 mm, and ø7.49 mm were used to conduct eddy current testing on artificially grooved fastener holes, and the influencing rules of aperture gap on eddy current testing signal were analyzed and summarized. The results showed that the amplitude of eddy current impedance decreased as the increase of aperture gap, which might be related to the lift-off effect. To ensure the stability and reliability of the eddy current testing signal, the aperture gap should be controlled within 0.33 mm for Ti-6Al-4V titanium alloy and 4340 steel.
  • LI Chunhui, ZHANG Congyi, YUAN Xiaodong, LIN Ziguo ZHOU Yu, ZHANG Jiaqi, FANG Junji, LIU Pan
    Physics Examination and Testing. 2026, 44(1): 54-58. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250019
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    The phase transformation point is a key parameter in the heat treatment and hot working processes of titanium alloys, and its accurate determination is of great significance for ensuring the material performance and process stability. According to the standard of HB 6623.1-1992, with TA1 titanium alloy as the research object, the synchronous thermal analyzer was used to investigate the effects of test times, sample mass, heating rate and crucible type on the determination of the phase tranformation point of titanium alloy by differential scanning calorimetry. It was showed that the measured phase transformation point gradually decreased with a increase of test times and eventually stabilized. An increase in sample mass and heating rate would both lead to a significant rise in the measured phase transformation point. However, the crucible type had no significant effect on the determination of phase transformation point.
  • Defect Analysis
  • DUAN Heng, HUANG Lixin
    Physics Examination and Testing. 2026, 44(1): 59-66. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250013
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    In order to investigate the failure mechanism of MJ thread of 15-5PH stainless steel, a pressure pulse test bench was set up to conduct pressure pulse tests on the retraction and extension actuating cylinder. The thread fracture causes were analyzed through means such as chemical composition analysis, hardness testing, and scanning electron microscope (SEM) inspection of the piston rod. The fatigue life of the MJ thread was evaluated by the joint simulation of Ansys and nCode. The notch concentration factor was introduced, and a fatigue life prediction method for MJ thread based on notch concentration factor was proposed. The results showed that the chemical composition and hardness test results of the sample all meet the requirements specified in the standard for 15-5PH stainless steel. The second thread at the bottom of the internal thread of piston rod had the maximum principal stress and the maximum plastic strain, and the shortest fatigue life, which was consistent with the failure results of engineering thread. The observation of fracture morphology indicated that the fatigue crack source originated from the internal thread of piston rod, and the crack rapidly propagated along the root of the thread. In the crack propagation zone, fatigue striations, river patterns and secondary cracks could be observed. In the instantaneous fracture zone, a large number of dimples could be observed. Finally, the introduction of notch concentration factor could quickly and accurately evaluate the fatigue life at the thread, providing certain engineering reference for the fatigue life prediction of MJ connection thread of actuating actuator.
  • MAO Li, LIU Kexiu, FENG Xiaoliang, MO Yingxiang
    Physics Examination and Testing. 2026, 44(1): 67-72. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250029
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    Aiming at the cracking problem of G102+TP347H dissimilar steel welded joint in the rear platen superheater tube of power plant boilers, the failure causes of the welded joint were analyzed through macroscopic observation, chemical composition analysis, microstructure analysis, the fracture morphology of scanning electron microscope(SEM), and micro-zone composition analysis, providing theoretical support for the safe and stable operation of power station boilers. The results showed that under high-temperature, high-pressure conditions and thermal stress, carbon migration at the fusion line on the G102 side of the dissimilar steel welded joint of the pipe sample formed a carburized layer. This caused abnormal mechanical properties and intergranular microcracks at the fusion line, ultimately leading to penetrating cracks at the fusion line on the G102 side. At the same time, the difference in thermal expansion coefficients and the thermal fatigue cycles accelerated the initiation and expansion of intergranular microcracks. It is recommended to optimize the welding process, reduce on-site welding, and strengthen inspection and examination.
  • REN Genzhu, CHEN Tianjiao, WANG Qingjun
    Physics Examination and Testing. 2026, 44(1): 73-78. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240099
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    The delayed fracture problem of prestressed concrete(PC) steel bar during processing and on pipe pile could cause losses to the manufacturers and users of PC. Therefore, the analysis and control of brittle fracture for PC steel bar have received extensive attention. Through macroscopic observation, metallographic structure, inclusion and fracture surface analysis of the brittle fracture samples of 30MnSi steel bar used in PC where low-stress fracture occurred, it was clarified that the scar defects on the surface of original wire rod were the direct cause of brittle fracture. Further analysis of the scar defects suggested that the surface crack defects of cast billet were the fundamental cause for the brittle fracture of steel bar. Through further optimization of the smelting and processing processes, the problem of brittle fracture in PC steel bar was effectively solved.
  • Subject Discussion
  • CAO Dan, WANG Jiarui, QU Peng, SUN Mingdao
    Physics Examination and Testing. 2026, 44(1): 79-85. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250070
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    The metallographic microstructure is of great significance for analyzing the types and properties of metal materials. This article mainly introduces the object detection methods of metallographic microstructure, the application of image segmentation technology in metallographic microstructure, and the development history of object detection algorithms. A detailed analysis was conducted on the evolution and advantages and disadvantages of convolutional neural network(CNN), region-based convolutional neural network(R-CNN), and Fast region-based convolutional neural network(Fast R-CNN) series algorithms, as well as several typical YOLO series algorithms. The performances of R-CNN series network models were compared with several typical YOLO series network models. The R-CNN series algorithms and YOLO series algorithms were compared and improved for the study of metallographic microstructure images. Finally, the development of object detection technology in the direction of metallographic microstructure images was discussed.
  • YU Qingkai, DING Chen, ZHANG Ke, ZHANG Liang, TANG Lingtian, ZHANG Jianwei
    Physics Examination and Testing. 2026, 44(1): 86-89. https://doi.org/10.13228/j.boyuan.issn1001-0777.20240110
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    This article objectively reflects the domestic laboratories testing level of eddy current method for determining coating thickness, helping laboratories identify the problems existing in daily testing. A systematic assessment and technical analysis were conducted on the laboratories results of proficiency testing scheme for determining coating thickness by eddy current method. Firstly, z-score statistical method was adopted to analyze the results of coating thickness on aluminum alloy substrates using eddy current method submitted by the laboratories, in order to evaluate its accuracy. Among 22 participating laboratories,19 laboratories obtained satisfactory result,1 laboratory had problem results, and 2 laboratories had unsatisfactory results. Then, various factors affecting the experimental results were discussed. Through the implementation of this proficiency testing scheme, it is conducive to further improving the internal quality control of laboratories and enhancing the testing level. At the same time, it provides an important basis for the supervision of laboratory certification and accreditation management departments in this field, and promotes the technological progress and development of the entire industry.
  • ZHU Xuesen, ZHOU Xiaoyu, ZHAO Yi
    Physics Examination and Testing. 2026, 44(1): 90-94. https://doi.org/10.13228/j.boyuan.issn1001-0777.20250008
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    Quartz vibrating beam accelerometer (VBA) is one of key components in aerospace field, and the measurement accuracy of its frequency signal directly affects the accuracy of motion acceleration determination. In response to the issues of low efficiency and severe signal crosstalk in existing multi-channel frequency testing methods for VBA, a frequency testing and switching system based on tree structure was proposed in this paper. This system achieved the isolation of high-density circuit board(PCB) partitioned common ground and tree-path isolation through self-locking relay network, and its performance was verified with double-blind testing. The experimental results showed that the system signal offset had decreased by 75% (from 41 μHz to 10 μHz) with changing from linear structure to tree structure, the crosstalk suppression ratio had increased by 15 dB, and the test efficiency of 72 channels had increased by 3.2 times. This design provides an efficient and low-interference solution for multi-channel VBA testing, offering practical value for engineering applications.