Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography
Jian Zhu1, Zhi-hao Zhang1,2, Jian-xin Xie1,2
1 Institute for Advanced Materials and Technology, University of Science and Technology Beijing, Beijing 100083, China; 2 Key Laboratory for Advanced Materials Processing (MOE), University of Science and Technology Beijing, Beijing 100083, China
Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography
Jian Zhu1, Zhi-hao Zhang1,2, Jian-xin Xie1,2
1 Institute for Advanced Materials and Technology, University of Science and Technology Beijing, Beijing 100083, China; 2 Key Laboratory for Advanced Materials Processing (MOE), University of Science and Technology Beijing, Beijing 100083, China
摘要 Based on the parent austenite orientation reconstruction method, it is aimed to reveal the origination of high angle grain boundaries (HAGBs) and its relationship with ductility of H13 steel. The orientation relationship between martensite andparent austenite of quenched H13 samples was (123.5°, 9.3°, 192.5°), which agreed with the Kurdumov–Sachs relationship.The variant distribution of quenched samples was dominated by close-packed plane group, and its high length fraction ofV1/V2 inter-variant boundaries of calculated 62.6% was mainly contributed to HAGBs (>45°). When the quenched H13samples underwent the pre-tempering treatment, their density of HAGBs (>45°) notably increased from 1.33 to 2.39l m-1, which improved its total elongation from 8.3% to 11.5%. Compared with the quenched H13 samples, the length fraction of V1/V2 inter-variant boundaries of H13 samples with pre-tempering for 5, 10 and 60 min was reduced by 6.7%,7.0% and 7.5%, respectively. During pre-tempering treatment, V1/V3&V5 variant pairs, etc., merged V1/V2 variant pairby strain-induced grain boundary migration, which decreased the length fraction of V1/V2 inter-variant boundaries by7.0%. The pre-tempering treatment significantly increased HAGBs (>45°) of H13 samples by sub-grains coarsening andstrain-induced grain boundary migration mechanism.
Abstract：Based on the parent austenite orientation reconstruction method, it is aimed to reveal the origination of high angle grain boundaries (HAGBs) and its relationship with ductility of H13 steel. The orientation relationship between martensite andparent austenite of quenched H13 samples was (123.5°, 9.3°, 192.5°), which agreed with the Kurdumov–Sachs relationship.The variant distribution of quenched samples was dominated by close-packed plane group, and its high length fraction ofV1/V2 inter-variant boundaries of calculated 62.6% was mainly contributed to HAGBs (>45°). When the quenched H13samples underwent the pre-tempering treatment, their density of HAGBs (>45°) notably increased from 1.33 to 2.39l m-1, which improved its total elongation from 8.3% to 11.5%. Compared with the quenched H13 samples, the length fraction of V1/V2 inter-variant boundaries of H13 samples with pre-tempering for 5, 10 and 60 min was reduced by 6.7%,7.0% and 7.5%, respectively. During pre-tempering treatment, V1/V3&V5 variant pairs, etc., merged V1/V2 variant pairby strain-induced grain boundary migration, which decreased the length fraction of V1/V2 inter-variant boundaries by7.0%. The pre-tempering treatment significantly increased HAGBs (>45°) of H13 samples by sub-grains coarsening andstrain-induced grain boundary migration mechanism.
Jian Zhu,Zhi-hao Zhang,Jian-xin Xie. Relationship between martensite microstructure and ductility of H13 steel from aspect of crystallography[J]. Journal of Iron and Steel Research International, 2021, 28(10): 1268-1281.
2021, Vol. 28 
