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2011年 18卷 2期
刊出日期：2011-02-15
材料
工艺
工艺
1
TANG Xu-long,ZHANG Zuo-tai,GUO Min,ZHANG Mei,WANG Xi-dong
Viscosities Behavior of CaO-SiO2-MgO-Al2O3 Slag With Low Mass Ratio of CaO to SiO2 and Wide Range of Al2O3 Content
The present paper is aimed at recycling of coal ash and blast furnace slag to produce mineral wool. Considering the mineralogical constitutions of coal ash and blast furnace slag, the primary quaternary slag compositions of CaO-SiO2-MgO-Al2O3 with basicity (mass ratio of CaO to SiO2) ranging from 05 to 09 and alumina ranging from 5% to 20% were investigated through a rotating cylinder method. The experimental results indicated that the viscosities decreased with increasing basicity above the liquidus temperature, and increased with increasing alumina content, and the maximum values were reached and as the alumina content was 20%, followed by the decrease with further increasing alumina content due to its amphoteric behavior. The amphoteric behavior of Al2O3 also performed in the relationship between viscosity and non-bridging oxygen per tetrahedrally-coordinated atom (NBO/T), and the viscosities decreased with increasing the NBO/T except the slag with a basicity 05 and Al2O3 20% which have a low NBO/T value and a low viscosity than others.-
2011 Vol. 18 (2): 1-6 [
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7
LI Hui-bin,WANG Hua,QI Yi-long,HU Jian-hang,LI You-ling,
Ilmenite Smelted by Oxygen-Enriched Top-Blown Smelting Reduction
Total ilmenite from Yunnan, China, difficult to smelt in blast furnace, was smelted by oxygen-enriched top-blown smelting reduction ironmaking technology. Much more details on smelting were discussed. Specifically, the influence of reduction temperature, slag basicity and molar ratio of carbon to oxygen on the reduction quality level including iron recovery and titanium and sulfur contents in the pig iron produced in the experiment was investigated. Iron recovery rate could reach 95% with titanium content below 005% in pig iron produced, under the conditions of holding time of 30 min at 1823 K, basicity of 11, carbon to oxygen molar ratio of 10 and oxygen-enriched flow rate of 250 L/h. Oxidization potential of top-space of smelting reduction vessel and slag combination could create the driving force to partition phosphorous, titanium and silicon into the slag, which ensured low contents of the impurities involved above and carbon in pig iron. In addition, it avoided the generation of Ti(C,N) that could reduce interfacial tension of slag, which induced the formation of foaming slag seriously. Furthermore, jam of chargings and bubble flooding would be triggered, resulting in deterioration of BF state, increase of iron loss and decline of desulfurization rate.
2011 Vol. 18 (2): 7-13 [
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14
JIANG Zhou-hua,LI Shuang-jiang,LI Yang
Thermodynamic Calculation of Inclusion Formation in Mg-Al-Si-O System of 430 Stainless Steel Melts
A phase diagram was drawn through thermodynamic calculation to understand the equilibrium conditions of 2MgO·SiO2, MgO·Al2O3, 3Al2O3·2SiO2, and 2MgO·2Al2O3·5SiO2 formation in Mg-Al-Si-O system of 430 stainless steel melts at 1873 K. Further, the thermodynamic formation and transformation conditions of MgO·Al2O3 inclusion were discussed. The following results are obtained when wSi=026% and wO=10×10-5 in molten steel. The uniphase cordierite inclusion is difficult to exist stably; MgO·Al2O3 inclusion cannot be formed in case of wAl being less than 1×10-6; 3Al2O3·2SiO2 would change to MgO·Al2O3 and 2MgO·SiO2 in turn with increasing the Mg content when wAl is above 17×10-6; with the formation of MgO·Al2O3 inclusion, Al content increases with increasing Mg content when wMg is over 17×10-9. For equilibrium condition and calculated steel composition, 2MgO·SiO2 inclusion would be formed ultimately and MgO·Al2O3 is almost inexistent.
2011 Vol. 18 (2): 14-17 [
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18
ZHOU Guo-ping,LIU Zhen-yu,YU Shi-chuan,CHEN Jun,QIU Yi-qing,WANG Guo-dong
Formation of Phosphorous Surface Inverse Segregation in Twin-Roll Cast Strips of Low-Carbon Steels
The formation of phosphorous surface inverse segregation (SIS) in twin-roll cast strips of low-carbon steels was studied. High phosphorous strips were fabricated by using a pilot twin-roll strip caster and a melt/substrate contacting apparatus, respectively. Solidification structures of strips were observed and analyzed, and phosphorus distributions along longitudinal sections of strips were investigated and discussed. The results showed that solidification structures of all strips were columnar grains, either integrated or coarse in the strip made by the melt/substrate contacting apparatus or damaged in some degree in cast strips; and that during cast strip solidification, enrichment of phosphorus occurred between columnar grains, and the average phosphorus concentration near the surface in the strip with 015% of phosphorus was measured to be about 027% which was obviously higher than that in the bulk.
2011 Vol. 18 (2): 18-23 [
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24
LI Pei-song,LU Jun-hui,QIU Sheng-tao,WANG Zhong-ying,ZHAO Pei
Control of Equiaxed Crystal Ratio of High Carbon Steel Billets by Circular Seam Cooling Nozzle
A circular seam cooling nozzle and its online control system have been developed to reduce the center segregation in high carbon steel billets by decreasing the superheat of the molten steel and improving the equiaxed crystal ratio based on the numerical results. An industrial experiment has been carried out on a 150 mm×150 mm caster to investigate the effect of the circular seam cooling nozzle on the superheat removal of the molten steel. The results show that the circular seam cooling nozzle can be used to control the casting temperature in a closed loop control system. The online control system can be effectively adapted to the variation of operating parameters. The casting lasts about 4 h and about 400 t steel is successfully produced in a continuous operation. The removal of about 14 ℃ superheat and the improvement of approximate 10% equiaxed crystal ratio can be achieved by the newly developed circular seam cooling nozzle.
2011 Vol. 18 (2): 24-30 [
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31
YU Hui,DU Feng-shan,XU Zhi-qiang
Influence of Pass Parameters on Retained Mandrel Rolling Process
Roller pass is one of the key factors affecting the product quality in the retained mandrel rolling process. The metal flow condition of rolling deformation area was researched using the FEA (finite element analysis) software Marc. The influences of the pass bottom radius, the sidewall radius, the sidewall angle, the roller shoulder fillet radius, as well as the roller gap on the rolling process under the conditions of different friction were discussed. Based on these results, the changes of the workpiece exit width, the mandrel axial force, the rolling force, and the rolling torque associated with various parameters were determined, which would provide the basis for designing the pass and determining the rolling condition reasonably.
2011 Vol. 18 (2): 31-37 [
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材料
38
WEN Bin,,SONG Bo,,PAN Ning,,SHU Qi-feng,, HU Xiao-jun,,MAO Jing-hong
Influence of Ce on Characteristics of Inclusions and Microstructure of Pure Iron
The experiments on adding Ce, Mn and S to molten iron have been carried out by means of the electric furnace, and the concentration of oxygen, the evolution of inclusions and microstructures of samples are analyzed, indicating that the concentration of dissolved oxygen decreases greatly after adding Ce. The calculated thermodynamics results at 1273 K performed on Factsage show that Ce2O2S and CeAlO3 are formed with the increase of Ce content for w(Ce)＞00002 and w(S)＜00001, while three cerium sulphides (CeS, Ce3S4 and Ce2S3, in sequence), MnS and Ce2O2S are formed with the increase of S content and the decrease of Ce content for w(Ce)＞00002 and w(S)＞00001. These results are consistent with the SEM observations. Finally, some possible reasons are given to explain the formation of intragranular ferrite in the pure iron.
2011 Vol. 18 (2): 38-44 [
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45
XIE Zhi-xiong,GAO Hai-yan,WANG Jun,YU Yan,FANG Yuan,SUN Bao-de
Static Recrystallization Behavior of Twin Roll Cast Low-Carbon Steel Strip
The static recrystallization kinetics of low-carbon steel cast strip was investigated by means of interrupted hot tensile tests. As-cast strip was reheated and soaked and its austenite grain size was similar to the width level of the as-cast columnar structure. The tests were carried out on Gleeble-3500 thermomechanical simulator. The deformation temperature is in the range of 800 to 1200 ℃ with strain rate of 001 to 1 s-1. The prestrain is fixed at 004 to 012, and the inter-hit delay time varies from 1 to 3000 s. Effect of deformation conditions and initial microstructure on static recrystallization behavior was investigated. The activation energy (Qsrx) and Avrami exponent (n) of static recrystallization were determined to have 241 kJ/mol and 054 respectively by linear regression of the experimental results. A kinetics model was proposed to describe the static recrystallization kinetics in low-carbon steel cast strip. The predicted softening fractions are in good agreement with the experimental results, indicating that the proposed equations can give an accurate estimate of the softening behaviors for the low-carbon steel cast strip.
2011 Vol. 18 (2): 45-51 [
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52
Amir Kalantari,Maziyar Azadbeh
Effect of Intermediate Annealing Temperature on Response of Repressing to Densification of Pre-Alloyed Cr-Mo Steel
Increasing density is one of the important factors for producing high quality powder metallurgy (PM) parts, which has beneficial effect on mechanical properties. One of the common techniques for achieving this goal is double compacting, which seems to be a potentially attractive method in PM route, also for Cr-Mo alloyed-steels. The objective of this research was to investigate the effect of first compacting pressure and intermediate annealing temperature on attaining higher densities and minimum interconnected porosity for Cr-Mo pre-alloyed steel. The effect of mentioned parameters was studied by measuring density, transverse rupture strength and macrohardness of repressed samples. The results show that for each first compacting pressure, the density range of repressed samples increases with the increasing annealing temperature up to a certain limit, due to C dissolution which causes free porosity and further densification. Annealing temperatures higher than optimum one should be avoided, since too much carbon dissolution results in harder and less deformable compacts. On the other hand, with regard to repressed density and other resulted properties, the amount of first compacting pressure offers considerable advantage in obtaining higher level of density and consequently improved mechanical properties.
2011 Vol. 18 (2): 52-56 [
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57
LAN Liang-yun,QIU Chun-lin,ZHAO De-wen,GAO Xiu-hua
Microstructural Evolution and Mechanical Properties of Nb-Ti Microalloyed Pipeline Steel
The correlation between microstructures and mechanical properties of a Nb-Ti microalloyed pipeline steel was investigated. The results revealed that with decreasing the finish rolling temperature and the cooling stop temperature, the matrix microstructure was changed from quasi-polygonal ferrite to acicular ferrite, as a result of improvement of both strength and low temperature toughness. By means of electron backscattered diffraction observation, an effective acicular ferrite packet contained several low angle boundaries or subboundaries plates which made important contributions to improvement of strength. It was found that many fine quasi-polygonal ferrite grains with high angle boundaries as the toughening structure were introduced into the acicular ferrite matrix to refine effective grain size and improve the toughness.
2011 Vol. 18 (2): 57-63 [
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YU Wei,QIAN Ya-jun,WU Hui-bin,YANG Yue-hui
Effect of Heat Treatment Process on Properties of 1000 MPa Ultra-High Strength Steel
Two types of steel, C-Mn-Cr-Mo-B microalloyed steel and C-Mn-Mo-Nb-Cu-B microalloyed steel, are designed to develop 1000 MPa ultra-high strength steel. Two kinds of processes, thermomechanical controlled process (TMCP) combined with traditional off-line quenching and tempering (QT) process versus controlled rolling process (CR) combined with direct quenching and tempering (DQ+T) process, are applied. The effect of heat treatment processing mode on the microstructure and mechanical properties is studied. The relationship between microstructure and mechanical properties is investigated by SEM and TEM. After tempering at 450 to 550 ℃ for 1 h, the steel produced by TMCP+QT process shows combination of excellent strength and low temperature toughness. The yield strength is above 1000 MPa, elongation above 15% and impact energy at -40 ℃ more than 30 J. After tempering at 450 ℃, a large number of ε-Cu particles precipitated in C-Mn-Mo-Nb-Cu-B steel produced by CR+DQ+T process lead to a significant increase in yield strength. And after tempering at 500 to 600 ℃, the yield strength of the steel is further improved to 1030 MPa because of precipitates, such as nitride or carbide of niobium, carbide of molybedenum and vanadium. When the tempering temperature is increased above 620 ℃, the yield strength is still higher than 1000 MPa and elongation is above 20% and impact energy at -40 ℃ is more than 35 J. After tempering at above 500 ℃, the toughness of the steel treated by TMCP+QT process is superior to that of steel by CR+DQ+T process.
2011 Vol. 18 (2): 64-69 [
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LI Yang,,LU Yu-peng,,WANG Chong,,LI Shi-tong,,CHEN Lu-bin,
Phase Stability of Residual Austenite in 60Si2Mn Steels Treated by Quenching and Partitioning
The residual austenite and its stability in commercial 60Si2Mn steel treated by quenching and partitioning (Q-P) were investigated. The Q-P heat treatment was carried out using a system of ordinary electric furnace—oil bath box—electric furnace. Cryogenic treatments at different temperatures were performed to assess the thermal stability of residual austenite. The microstructure, particularly residual austenite, was analyzed using optical microscope and X-ray diffraction (XRD), and the microhardness and Rockwell hardness were measured. The residual austenite with the volume fraction as much as 137% and the HRC hardness level of 41 were achieved, and the residual austenite is relatively stable.
2011 Vol. 18 (2): 70-74 [
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YANG Min,SONG Chang-jiang,DAI Yong-xiang,ZHU Liang,LI Ke-feng,ZHAI Qi-jie
Microstructural Evolution of Gas Atomized Fe-25Cr-32C Alloy Powders
The microstructural evolution of the gas atomized Fe-25Cr-32C powders was investigated by using optical microscope, scanning electron microscope, and X-ray diffraction. The experimental results showed that the atomized Fe-25Cr-32C powders were mainly composed of austenite and (Fe,Cr)7C3 carbide. Eutectic microstructure was developed in the larger particles, whereas dendritic microstructure was obtained in the particles with diameter less than 38 μm. The reason for microstructure change should be the difference of nucleation undercooling for particles.
2011 Vol. 18 (2): 75-78 [
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