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Determination of phase transformation point of TA24 alloy by composition calculating method and differential scanning calorimetry |
LI Chunhui1, ZHANG Congyi1, WANG Shuo1, CHEN Jieming1, LIU Pan1,2,3, ZHANG Xinyao1,3,4 |
1. Luoyang Ship Material Research Institute, Luoyang 471023, China; 2. National New Material Production and Application Demonstration Platform (Advanced Marine Engineering and High-tech Ship Materials), Luoyang 471023, China; 3. State Key Laboratory for Marine Corrosion and Protection, Luoyang 471023, China; 4. Henan Key Laboratory of Technology and Application of Structural Materials for Ship and Marine Equipment, Luoyang 471023, China |
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Abstract The β transformation temperatures of 11 pieces of TA24 near α titanium alloy samples in 4 specifications were measured by composition calculating method and differential scanning calorimetry. In the composition calculating method, the β transformation temperature of titanium alloy was determined according to the contribution rate of alloying elements and impurity elements to the phase transformation temperature. In the differential scanning calorimetry, the β transformation temperature was measured based on the heat change of titanium alloy during phase transition. The results showed that under the condition of 95% confidence, the deviation between methods was (-1.3±5.8) ℃, and the absolute value of deviation was (2.4 ± 3.9) ℃. The measurement results of composition calculating method and differential scanning calorimetry method were consistent, and the deviation was between -6.9 ℃ and 2.4 ℃, which were both less than the allowable deviation (±8 ℃) of two parallel tests in the laboratory specified by HB 6623.1-1992 and HB 6623.2-1992. The composition calculating method could be used as a convenient and effective method to quickly predict the β transformation temperature of TA24 titanium alloy.
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Received: 26 May 2023
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