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二次淬火温度对18Cr2Ni4WA钢高温渗碳层组织及强塑性影响

Effect of secondary quenching temperature on microstructure and strength-ductility of high-temperature carburized layer in 18Cr2Ni4WA steel

  • 摘要: 18Cr2Ni4WA钢经渗碳处理后具有高表面硬度和良好的心部承载能力,广泛应用于重载传动齿轮等关键部件。传统930 ℃渗碳工艺存在生产周期长和能耗高的问题。高温渗碳可显著提高钢的渗碳效率,但同时易引起残余奥氏体含量升高及碳化物形态失衡,从而削弱渗碳层的力学性能。针对上述问题,本文采用950 ℃高温渗碳工艺,并通过调控二次淬火温度为775、800、825、850 ℃,系统研究其对18Cr2Ni4WA钢渗碳层组织演变及强塑性匹配的影响。结果表明,随着二次淬火温度升高,原奥氏体晶粒尺寸由7.05 μm增大至12.58 μm,由大角度晶界界定的马氏体结构单元尺寸(即马氏体的有效晶粒尺寸)由1.53 μm增大至2.18 μm,渗碳层中残余奥氏体体积分数由8.6%升高至12.1%。775 ℃二次淬火条件下,渗碳层中存在连续网状碳化物,易诱发沿晶开裂。当淬火温度提高至800 ℃时,网状碳化物连续性被有效破坏,显著提升了材料塑性。相比之下,进一步提高淬火温度会导致晶粒粗化及残余奥氏体增多,材料伸长率明显下降。综合组织与性能分析,800 ℃二次淬火试样获得最佳强塑性匹配,其断裂伸长率为4.6%,强塑积达到7.5 GPa·%。研究结果为高温渗碳18Cr2Ni4WA钢的后续热处理工艺优化提供了试验依据。

     

    Abstract: After carburizing treatment, 18Cr2Ni4WA steel exhibits high surface hardness and good core load bearing capacity, making it widely used in key components such as heavy load transmission gears. The traditional carburizing process at 930 ℃ has the problems of long production cycle and high energy consumption. High temperature carburizing significantly improves carburizing efficiency of steel, but it also tends to cause an increase in retained austenite content and an imbalance in carbide morphology, thereby weakening the mechanical properties of the carburized layer. To address these issues, this study adopted a high temperature carburizing process at 950 ℃ and systematically investigated its effect on the microstructure evolution and strength-ductility matching of the carburized layer in 18Cr2Ni4WA steel by adjusting the secondary quenching temperature of 775, 800, 825, 850 ℃. The results show that as the secondary quenching temperature increases, the prior austenite grain size grows from 7.05 μm to 12.58 μm, the size of martensite structural units delimited by high angle grain boundaries (i.e., the effective grain size of martensite) increases from 1.53 μm to 2.18 μm, and the retained austenite volume fraction in the carburized layer rises from 8.6% to 12.1%. Under the secondary quenching condition at 775 ℃, continuous network carbides exist in the carburized layer, which easily induce intergranular cracking. When the quenching temperature is raised to 800 ℃, the continuity of the network carbides is effectively broken, significantly improving the ductility of the material. In contrast, further increasing the quenching temperature leads to grain coarsening and an increase in retained austenite, resulting in a marked decrease in the elongation of the material. Based on comprehensive microstructure and property analysis, the sample quenched at 800 ℃ achieves the best strength-ductility matching, with a fracture elongation of 4.6% and a strength-ductility product of 7.5 GPa·%. These findings provide an experimental basis for optimizing the subsequent heat treatment process of high-temperature carburized 18Cr2Ni4WA steel.

     

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