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冷轧形变量对Fe-35Mn-8Al-0.3C轻质钢超塑性组织和力学性能影响

Effect of cold rolling reduction on superplastic microstructure and mechanical properties of Fe-35Mn-8Al-0.3C low-density steel

  • 摘要: 以5 mm厚热轧板为初始材料,经冷轧变形至不同形变量(60%、80%、90%、94%和96%)后,在800 ℃、1×10-2 s-1条件下进行高温拉伸试验,并结合扫描电镜(SEM)、电子背散射衍射(EBSD)、透射电镜(TEM)等表征手段分析组织-性能演变,以探究冷轧变形量对Fe-35Mn-8Al-0.3C低密度钢超塑性的影响。高温拉伸结果表明,所有冷轧样品(形变量60%~96%)在高温拉伸条件下均获得超过300%的伸长率,呈现典型超塑性特征;随形变量增加,伸长率由60%冷轧板的341%逐渐上升,最高达94%冷轧板的612.5%。组织表征发现,高温拉伸过程中发生Mn元素再配分与动态再结晶,使初始冷轧α+γ双相带状组织转变为富Mn的β-Mn与γ相“互嵌”的双相等轴晶组织;随冷轧形变量增大,高温拉伸后的动态再结晶体积分数由79.6%增至99%,但β-Mn与γ两相体积分数接近,晶粒尺寸稳定在1~2 μm,组织基本不受初始形变量影响。超塑性变形后,硬相β-Mn为完全再结晶结构,而软相γ中仍保留高密度位错。基于上述研究,确定冷轧形变量为90%~94%时可获得约600%伸长率的预变形工艺,并提出低密度钢的超塑性变形机制为γ相位错滑移辅助与晶界/相界滑动共同主导。

     

    Abstract: Using a 5-mm-thick hot-rolled plate as the starting material, specimens were cold-rolled to various reductions (60%, 80%, 90%, 94% and 96%) and subsequently subjected to high-temperature tensile testing at 800 ℃ and 1×10-2 s-1. Scanning electron microscopy, electron backscatter diffraction, and transmission electron microscopy were employed to characterize the microstructure-property evolution, aiming to clarify the effect of cold rolling reduction on the superplasticity of Fe-35Mn-8Al-0.3C low-density steel. The high-temperature tensile results show that all cold-rolled samples (with reductions of 60%-96%) exhibit elongations exceeding 300% under the tested conditions, demonstrating typical superplastic behavior. With increasing reduction, the elongation gradually rises from 341% for the 60% cold-rolled sheet to a maximum of 612.5% for the 94% cold-rolled sheet. Microstructural characterization reveals that Mn redistribution and dynamic recrystallization occur during high-temperature tensile deformation, transforming the initial cold-rolled α+γ dual-phase banded structure into an equiaxed dual-phase structure consisting of Mn-rich β-Mn and γ phases in an interlocked configuration. As the cold rolling reduction increases, the fraction of dynamic recrystallization after high-temperature tension rises from 79.6% to 99%, while the volume fractions of β-Mn and γ phases remain comparable and the grain size stabilizes at 1-2 μm, indicating that the final microstructure is largely independent of the initial reduction. After superplastic deformation, the hard β-Mn phase exhibits a fully recrystallized structure, whereas the soft γ phase retains a high density of dislocations. Based on these findings, a pre-deformation process with a cold rolling reduction of 90%-94% is identified as capable of yielding approximately 600% elongation, and the superplastic deformation mechanism of the low-density steel is proposed to be jointly governed by dislocation slip in the γ phase and grain boundary/phase boundary sliding.

     

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