氮化硅陶瓷夹具的设计及其在陶瓷基复合材料高温力学性能测试中的应用
Design of silicon nitride ceramic fixture and its application in high-temperature mechanical property testing of ceramic matrix composites
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摘要: 由于高温环境下夹具材料强度不足及试样构型不兼容的双重制约,使得适配陶瓷基复合材料(CMCs)高温力学性能测试的夹具材料选择与结构设计成为热点。本文选择高温环境下能保持优异的耐高温性能、力学性能和相结构稳定性的Si3N4陶瓷作为夹具材料,设计并制备了适配燕尾型板状CMCs的高温夹具,并验证了其在1 000 ℃环境下CMCs力学性能检测中的应用可行性。选用Abaqus有限元分析软件对Si3N4陶瓷夹具和碳化硅复合材料进行了热应力分布和受力状态分析,结果表明,通过创新性的燕尾型试样夹持结构结合倒角应力释放设计,显著降低了夹具薄弱区的应力集中,同时在高温服役环境下,夹具拥有良好的载荷传导和抗失效性能。1 000 ℃环境下,CMCs的高温拉伸和高温疲劳性能测试结果表明,该夹具在高温下具有稳定的力学响应和耐用性。Abstract: Due to the dual constraints of insufficient strength of fixture materials in high-temperature environments and the incompatibility of sample configurations, the selection of fixture materials and the structural design for the high-temperature mechanical property testing of ceramic matrix composites (CMCs) have become a hot topic. Si3N4 ceramics with excellent high-temperature resistance, mechanical properties and phase structure stability under high-temperature conditions were selected as the fixture material. A high-temperature fixture suitable for the dovetail-shaped plate-like CMCs was designed and fabricated, and its feasibility in the mechanical property testing of CMCs at 1 000 ℃ was verified. The thermal stress distribution and stress state of Si3N4 ceramic fixture and silicon carbide composite were analyzed by Abaqus finite element analysis software. The results showed that the stress concentration in the fixture weak area was significantly reduced by combining the innovative dovetail-shaped sample clamping structure with the chamfered stress release design. Moreover, the fixture exhibited excellent load conduction and failure resistance property in the high-temperature service environment. The test results of high-temperature tensile and high-temperature fatigue properties of CMCs at 1 000 ℃ indicated that this fixture exhibited stable mechanical response and durability at high-temperatures.
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