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热等静压对K447A/DD412双合金组织的影响

Effect of hot isostatic pressing on the microstructure of K447A/DD412 bimetal

  • 摘要: 针对目前等轴晶/单晶双合金高温合金研究匮乏的问题,本文采用二次浇注法成功制备了K447A/DD412双合金双性能试棒,并研究了热等静压(HIP)对其组织的影响。铸态组织分析表明,两种合金之间存在一个较宽的过渡区,且未发现界面氧化现象,因而具有良好的冶金结合。双合金双性能试棒整体组织可分为4个区域:K447A、DD447、成分过渡区(CTZ)和DD412,各区域显示出显著的成分和组织差异,表现为共晶和碳化物面积分数从K447A到DD412逐渐减少,而枝晶干γ′相面积分数逐渐增加。经热等静压后,显微组织中的疏松和微孔基本得到消除,共晶和碳化物面积分数整体下降,但形貌变化不显著。此外,枝晶干γ′相形貌得到改善,面积分数有所升高。应该指出,热等静压态的组织仍然存在γ′相尺寸较大等问题,需要通过后续固溶和时效热处理进一步优化。本研究为双合金双性能高温合金整体叶盘的发展提供了理论与实验基础。

     

    Abstract: Given the current lack of research on equiaxed/single crystal bimetal superalloys, K447A/DD412 dual-alloy dual-property test bars were successfully fabricated via a secondary pouring process in this study. The effect of hot isostatic pressing(HIP) on their microstructure was investigated. Analysis of the as-cast microstructure revealed a wide transition zone between the two alloys with no interfacial oxidation, indicating a good metallurgical bond. The overall microstructure of the bimetal test bar could be divided into four regions: K447A, DD447, a compositional transition zone(CTZ), and DD412. Significant compositional and microstructural differences were observed among these regions. The area fraction of eutectic and carbides gradually decreased from K447A to DD412, while the area fraction of the dendritic γ' phase increased correspondingly. After hot isostatic pressing treatment, microporosity was essentially eliminated. The area fraction of eutectic and carbides decreased overall, though their morphology did not change significantly. Additionally, the morphology of the dendritic γ' phase was refined, and its area fraction increased. It should be noted that the HIP-treated microstructure still exhibited issues such as excessively large γ' phase size, which requires further optimization through subsequent solution and aging heat treatments. This study provides a theoretical and experimental basis for the development of dual-alloy dual-property blisks.

     

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