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退火工艺对DR材显微组织和力学性能的影响

Influence of continuous annealing process on the microstructure and mechanical properties of double-reduced tin plate

  • 摘要: 为提升DR材成形性能,本文对比了α相再结晶退火和α+γ两相区退火两种不同退火工艺对一种高强DR材组织和性能的影响,通过激光共聚焦显微镜、SEM、TEM观察了样品显微组织,采用洛氏硬度计检测了样品表面硬度,采用拉伸试验机检测了样品力学性能。结果表明,α相再结晶退火工艺下DR材显微组织为铁素体+渗碳体,铁素体晶粒尺寸差异较大,粗大渗碳体离散分布在铁素体晶内和晶界位置。α+γ两相区退火工艺下DR材显微组织为铁素体+珠光体,铁素体晶粒呈等轴状且尺寸分布均匀,珠光体岛分布在铁素体晶界位置,片层间距达到约150 nm。两种不同退火工艺下,DR材表面硬度均控制在(73±4)HR30T。相比α相再结晶区退火,α+γ两相区退火工艺下DR材表面硬度提高约1.5个单位,屈服强度Rp0.2提高约25 MPa,抗拉强度Rm提高约30 MPa,断后伸长率A50提高约4.0%。α+γ两相区退火工艺下,冷轧残留的粗大渗碳体得到充分回溶形成奥氏体,且在均热后的冷却转变中形成尺寸均匀的等轴铁素体晶粒和片层间距细小的珠光体球团,这是材料强度获得提高且塑性得到显著改善的主要原因。

     

    Abstract: In order to improve the plasticity of double-reduced tin plate,this paper studied the influence of α phase recrystallization annealing and α+γ phase intercritical annealing on the microstructure and mechanical properties of double-reduced tin plate, In this paper,the microstructures of the steel were detected by OM、SEM and TEM, the rockwell hardness and mechanical propertie of the material were tested respectively by rockwell hardness tester and tensile tester. The result showed that with the α phase recrystallization annealing process, the experimental steel′s microstructure were ferrite and cementite,the grain size of ferrite varied greatly and coarse cementite discretely distributed in ferrite grains and grain boundaries. With the α+γ phase intercritical annealing process, the experimental steel′s microstructure were ferrite and pearlite,the ferritic grains were equiaxed and distributed in uniform size,the pearlite island distributed in the ferrite grain boundary and the lamellar space of the pearlite reached about 150 nm.The rockwell hardness HR30T of double-reduced tin plate with those two different annealing processes were both controlled between (73±4)HR30T.Compared with the double-reduced tin plate processed with α phase recrystallization annealing,the rockwell hardness of double-reduced tin plate processed with α+γ phase intercritical annealing increased by about 1.5 units,the yield strength Rp0.2 increased by about 25 MPa, the tensile strength Rm increased by about 30 MPa, and the elongation A50 increased by about 4.0%.With the α+γ phase intercritical annealing process, the coarse cementite residued from the cold rolling redissolved sufficiently and thus formed equiaxed ferrite grains distributed in uniform size and pearlite with fine layer space during the subsequently cooling process after soaking heat, which led to the significant improvement of the material′s strength and plasticity.

     

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