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2012年 19卷 3期
刊出日期：2012-03-15
材料
工艺
工艺
1
WANG Yu-nan,BAO Yan-ping,CUI Heng,CHEN Bin,JI Chen-xi
Final Temperature Prediction Model of Molten Steel in RH-TOP Refining Process for IF Steel Production
In order to precisely control the final temperature of molten steel in RH (Ruhrstahl Heraeus)-TOP blowing refining, the final temperature prediction models of molten steel in RH-TOP blowing refining process for Interstitial Free (IF) steel production were established under the condition of oxygen blowing and non-oxygen blowing respectively. The results show that the beginning molten steel temperature of refining and the amount of added scrap were influential factors, the baking temperature in vacuum chamber was a factor that had small influence. When the model was operated, the hitting probability was above 95% (under the condition of both oxygen blowing and non-oxygen blowing) of prediction deviation of ±10 ℃. The accuracy is analyzed.
2012 Vol. 19 (3): 1-5 [
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JIANG Mao-fa,CUI Yu-yuan,WANG De-yong,MIN Yi,LIU Cheng-jun
Effect of Modification Treatment for Reduction of Dephosphorization Slag in Hot Metal Bath
To extract the valuable elements from the steel slag, a novel approach has been proposed by modification treatment to provide the stronger driving forces and accelerate the reduction. Three types of dephosphorization steel slags were reduced using carbon-saturated iron bath to extract iron and phosphorus simultaneously. During the process of reduction, slag composition, temperature, and original P2O5 content were investigated respectively. Slag modification treatment, adding either silica or alumina to vary the slag composition, was proven to accelerate the reduction of dephosphorization slag. The equilibrium time can be shortened from 60 to 30 min. Slag modification also allowed the reduction reaction to occur at lower temperature. After slag modification, the original P2O5 content in slag presents a slight difference on reduction process. Almost half of the reduced phosphorus was vaporized within 5 and 20 min. As more and more FeO was reduced, CO gas generation decreased, and evaporation amount of phosphorus therefore decreases.
2012 Vol. 19 (3): 1-6 [
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6
HOU Yan-qing,XIE Gang,TAO Dong-ping,YU Xiao-hua,LI Rong-xing
Activity Calculation in Complex Metallurgical Molten Slag Systems Based on Regular Solution Model
The activity of FetO is very important in ironmaking and steelmaking process. In order to predict the activity of FetO and optimize the operation conditions in ironmaking and steelmaking process, by application of regular solution model in molten slag systems, FeO-Fe2O3-SiO2 ternary system, FeO-Fe2O3-SiO2-CaO and FeO-Fe2O3-SiO2-NiO quaternary systems have been studied by the chemical equilibrium between H2/H2O gas mixture and liquid slag contained in solid iron. The values of interaction energy between cations concerning steelmaking slags have been determined by application of ferric-ferrous iron equilibrium and iron-ferric iron equilibrium. And then the activity of FetO can be calculated. The results show that the relative error is 39% in FeO-Fe2O3-SiO2 system and 18% in FeO-Fe2O3-SiO2-CaO system. The prediction of activities of FetO in the systems are in good agreement with the measurements and the regular solution model is valid for predicting the activity of FetO in complex molten slags systems. The activity of FetO in FeO-Fe2O3-NiO system have not been tested presently, and the calculated result can not be assessed.
2012 Vol. 19 (3): 6-10 [
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11
F Farshidfar,M Ghassemi Kakroudi
Effect of Chromite-Silica Sands Characteristics on Performance of Ladle Filler Sands for Continuous Casting
Free opening rate is mainly determined by the performance of the ladle filler sand. High free opening rates of ladles are required in steel making to improve steel quality. Chromite ladle filler sands are one of the most widely used ladle filler sand. Several operative variables and materials characteristics affect the performance of the sands. Three sets of chromite ladle filler sands were selected and researches were focused on the sintering behaviour and performance of the sands under operative conditions. The effect of particle size distribution on sintering, microstructure, flowability, and permeability were presented. In all cases, the particle size varies from 01 to 15 mm corresponding to free flowing powders. One of the samples has higher permeability factor in comparison with others due to low particle size distribution. The other sample presents very good free opening due to its very good flowability and permeability factor.
2012 Vol. 19 (3): 11-13 [
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14
WANG Tao,XIAO Hong,ZHAO Tie-yong,QI Xiang-dong
Improvement of 3-D FEM Coupled Model on Strip Crown in Hot Rolling
In order to simulate and analyze hot strip crown and flatness accurately and efficiently, the 3-D (three-dimensional) coupled model involved in RPFEM (rigid-plastic finite element method) is improved based on the analytical model of forecasting rolling force distribution. In the analytical model, variational method is employed to solve the lateral flow of metal and influential function method is employed to calculate roll deflection, the lateral distribution of rolling force can be obtained rapidly by iterative strategy. Then the 3-D coupled model uses the result as initial distribution of rolling force to calculate roll deflection and makes the initial on-load roll gap profile close to the final value, so as to reduce iterations and increase efficiency. Compared with previous algorithms, the improved model can reduce the iterations by about 50% and shorten the computing time by about 60% on the basis of the calculation accuracy.
2012 Vol. 19 (3): 14-19 [
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ZHAO De-wen,ZHANG Shun-hu,LI Can-ming,SONG Hong-yu,WANG Guo-dong
Rolling With Simplified Stream Function Velocity and Strain Rate Vector Inner Product
The dual-stream function velocity field is reduced in order to analyze two-dimensional plate broadside rolling in roughing. The strain rate vector inner product and integral mean value theorem, as well as co-line vector inner product are used respectively in plastic deformation power, friction losses and shear power. A theoretical solution of roll torque and separating force for the rolling is obtained and the calculated results by the solution are compared with those measured in broadside rolling on-line. It shows that both the force and torque calculated are higher than those of measured, but the maximum relative error between them is no more than 11%.
2012 Vol. 19 (3): 20-24 [
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材料
31
SHAN Xiu-ying,,,LIU Hong-min,,JIA Chun-yu,,SUN Jian-liang,
Flatness and Profile Integration Control Model for Tandem Cold Mills
Using the effective matrix methods of flatness and profile control synthetically, the flatness and profile integration control scheme for tandem cold mills is built in order to increase flatness and profile control precision of tandem cold mills. Corresponding control strategies are adopted for various control objectives of different stands and the coordination control strategies of various stands are given, which makes the on-line flatness control cooperate with on-line profile control and implements the parallel control of different stands. According to the measured flatness and profile data of some 1550 mm tandem cold mills, the control scheme is verified and the result indicates that the scheme has high flatness and profile control precision with steady and reliable control process. A new way and method is supplied for researching shape control of tandem cold mills.
2012 Vol. 19 (3): 31-37 [
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LI Da-zhao,,WEI Ying-hui,HOU Li-feng,LIN Wan-ming
Microstructural Evolution of Surface Layer of TWIP Steel Deformed by Mechanical Attrition Treatment
A nanocrystalline layer was synthesized on the surface of TWIP steel samples by surface mechanical attrition treatment (SMAT) under varying durations. Microhardness variation was examined along the depth of the deformation layer. Microstructural characteristics of the surface at the TWIP steel SMATed for 90 min were observed and analyzed by optical microscope, X-ray diffraction, transmission and high-resolution electron microscope. The results show that the orientation of austenite grains weakens, and α-martensite transformation occurs during SMAT. During the process of SMAT, the deformation twins generate and divide the austenite grains firstly; then α-martensite transformation occurs beside and between the twin bundles; after that the martensite and austenite grains rotate to accommodate deformation, and the orientations of martensite and between martensite and residual austenite increase; lastly the randomly oriented and uniform-sized nanocrystalline layers are formed under continuous deformation.
2012 Vol. 19 (3): 38-46 [
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ZHANG Chao-lei,LIU Ya-zheng,ZHOU Le-yu,JIANG Chao
Secondary Hardening, Austenite Grain Coarsening and Surface Decarburization Phenomenon in Nb-Bearing Spring Steel
The secondary hardening, the austenite grain coarsening and the surface decarburization phenomenon of Nb-bearing spring steel were investigated, and the effects of niobium on tempered microstructure was studied using scanning electron microscope. The results show that the micro-addition of niobium increases the tempering resistance and produces secondary hardening. The effect of niobium on the size and distribution of cementite particles is one of the primary reasons to increase the hardness after tempering. The grain-coarsening temperature of the spring steel is raised 150 ℃ due to Nb-addition. Furthermore, both the secondary hardening and the austenite grain coarsening phenomenon congruously demonstrate niobium begins observably dissolving above 1100 ℃ in the spring steel. Besides, niobium microalloying is an effective and economy means to decrease the decarburization sensitivity of the spring steels.
2012 Vol. 19 (3): 47-51 [
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52
JIA Yue-cai,GUO Hai-rong,LI Ran,LI Hua-long
Effects of Rolling Processes on Yield Ratio and Formability of Hot Rolled Gas Cylinder Steel
Deep drawing properties of hot rolled gas cylinder steel was investigated by using HP295 steel in terms of microstructure, texture, yield ratio, plastic strain ratio (r-value) and plastic anisotropy (Δr). The grains in the hot strip were largely equiaxed, and the texture was weak, containing α- and γ-fibre. Reheating temperature, finish rolling temperature and cooling rate after rolling influenced the ferrite-pearlite band formation significantly, and the yield ratio increased steeply with decreasing coiling temperature below 630 ℃. The anisotropy is relatively high due to retained severe ferrite-pearlite band. A mechanism of the band formation due to manganese segregation is elaborated and confirmed validly, from which the measures to avoid the band formation are worked out. Rolling parameters have been optimized by the measures, and industrial production of the gas cylinder steel has been made possible with much improved r-and Δr-values, while meeting other specifications.
2012 Vol. 19 (3): 52-56 [
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MA Dang-shen,CHI Hong-xiao,,ZHOU Jian,YONG Qi-long,
Microstructure and Mechanical Properties of Martensitic Stainless Steel 6Cr15MoV
Martensitic stainless steel containing Cr of 12% to 18% (mass percent) are common utilized in quenching and tempering processes for knife and cutlery steel. The properties obtained in these materials are significantly influenced by matrix composition after heat treatment, especially as Cr and C content. Comprehensive considered the hardness and corrosion resistance, a new type martensitic stainless steel 6Cr15MoV has been developed. The effect of heat treatment processes on microstructure and mechanical properties of 6Cr15MoV martensitic stainless steel is emphatically researched. Thermo-Calc software has been carried out to thermodynamic calculation; OM, SEM and TEM have been carried out to microstructure observation; hardness and impact toughness test have been carried out to evaluate the mechanical properties. Results show that the equilibrium carbide in 6Cr15MoV steel is M23C6 carbide, and the M23C6 carbides finely distributed in annealed microstructure. 6Cr15MoV martensitic stainless steel has a wider quenching temperature range, the hardness value of steel 6Cr15MoV can reach to HRC 608 to HRC 616 when quenched at 1060 to 1100 ℃. Finely distributed carbides will exist in quenched microstructure, and effectively inhabit the growth of austenite grain. With the increasing of quenching temperature, the volume fraction of undissolved carbides will decrease. The excellent comprehensive mechanical properties can be obtained by quenched at 1060 to 1100 ℃ with tempered at 100 to 150 ℃, and it is mainly due to the high carbon martensite and fine grain size. At these temperature ranges, the hardness will retain about HRC 592 to HRC 616 and the Charpy U-notch impact toughness will retain about 173 to 20 J. A lot of M23C6 carbides precipitated from martensite matrix, at the same time along the boundaries of martensite lathes which leading to the decrease of impact toughness when tempered at 500 to 540 ℃. The M3C precipitants also existed in the martensite matrix of test steel after tempered at 500 ℃, and the mean size of M3C precipitates is bigger than that of M23C6 precipitates.
2012 Vol. 19 (3): 56-61 [
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ZHANG Yan,SUN Yu-fu,ZHAO Jing-yu,GUAN Shao-kang
Effects of Al on Microstructure and High-Temperature Wear Properties of Austenitic Heat-Resistant Steel
Microstructure and high-temperature dry sliding wear at 600 ℃ in ambient air of austenitic heat-resistant steel ZG40Cr25Ni20 with different contents (mass percent) of Al (0 to 710%) have been investigated. The results show that microstructures of 468% and 710% Al addition content consist of the matrix and reinforcement of intermetallic compound γ′ and carbide, while microstructures of ZG40Cr25Ni20 without Al and with Al of 168% are absent of γ′. Higher wear resistance than the original ZG40Cr25Ni20 alloy is achieved in alloys with higher content of Al under the same high-temperature wear test condition. The wear rates of Fe-25Cr-20Ni-710Al and Fe-25Cr-20Ni-468Al are only 2083% and 4583% of that of Fe-25Cr-20Ni, respectively. Heat-resistant steels with higher contents of Al (472% and 710%) have higher hardness than those with lower contents of Al (168% and 0). Wear mechanisms of ZG40Cr25Ni20 are considered as severe plough plastic deformation and slight adhesive. However, wear mechanisms of Fe-25Cr-20Ni-468Al are light micro-cutting and oxidation-wear, while that of Fe-25Cr-20Ni-710Al are severe adhesive transfer and oxidation-wear.
2012 Vol. 19 (3): 62-66 [
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ZHANG Jie,CAI Qing-wu,WU Hui-bin,ZHANG Kun,WU Bo
Effect of Tempering Temperature on Microstructure and Properties of E690 Offshore Plate Steel
A new kind of Mn-Mo-Nb-Cu-B bainite steel which satisfied mechanical demands of E690 offshore plate steel was designed. The effect of two processes——thermomechanical control process (TMCP)+tempering (T) and thermomechanical control process (TMCP)+reheating and quenching (RQ)+tempering (T)——on microstructure and mechanical properties were studied by means of scan electron microscope (SEM), transmission electron microscope (TEM) and electron back scatter diffraction (EBSD). The results showed that optimal mechanical properties were available when tempering at 550 ℃ for both processes. The microstructure of the TMCP+T treated sample tempering in the range of 450 to 550 ℃ for 1 h did not change dramatically yet the lath in the TMCP+RQ+T treated sample merged together and transformed into polygonal ferrite. At the same time, the sub-structure of grain bainite transformed from lath to cell-shape to refine grains with tempering temperature mounting. Lots of sub-grain boundaries were located within bainite and adjacent bainite grain boundaries were high angle.
2012 Vol. 19 (3): 67-72 [
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HAN Wei,MENG Xian-ming,ZHANG Jun-bao,ZHAO Jie
Elastic Modulus of 304 Stainless Steel Coating by Cold Gas Dynamic Spraying
304 stainless steel coating was deposited on the IF steel substrate by cold gas dynamic spraying (CGDS), and the elastic modulus of the 304 stainless steel coating was studied. The elastic modulus of cold sprayed 304 stainless steel coating was measured using the three-point bend testing and the compound beam theory, and the other mechanic parameters (such as the equivalent flexural rigidity and the moment of inertia of area) of the coatings were also calculated using this compound beam theory. It is found that the calculated results using the above methods are accurate and reliable. The elastic modulus value of the cold sprayed 304 stainless steel coating is 1179×105 MPa, and it is slightly lower than the 304 stainless steel plate (about 2×105 MPa). It indicates that the elastic modulus of the cold sprayed coatings was quite different from the comparable bulk materials. The main reason is that the pores and other defects are existed in the coatings, and the elastic modulus of the coatings also depends on varies parameters such as the feed stock particle size, porosity, and processing parameters.
2012 Vol. 19 (3): 73-78 [
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